1: triethylamine / H2O; acetone / 0 °C
2: NaN3 / H2O; acetone / 0.75 h / Ambient temperature
3: toluene / 0.5 h / Heating
4: Heating
5: LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Nichols, David E.; Lloyd, David H.; Hoffman, Andrew J.; Nichols, Maxine B.; Yim, George K. W.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 530 - 535
1: triethylamine / H2O; acetone / 0 °C
2: NaN3 / H2O; acetone / 0.75 h / Ambient temperature
3: toluene / 0.5 h / Heating
4: Heating
5: H2 / ethanol / 24 h / 1810.02 Torr
View Scheme
参考文献
Nichols, David E.; Lloyd, David H.; Hoffman, Andrew J.; Nichols, Maxine B.; Yim, George K. W.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 530 - 535
