54509-73-8合成路线 （共 3623 条）
反应条件
1: 1-bromo-4-ethenylbenzene; ethene With Na[B(3,5-(CF3)2C6H3)4] in dichloromethane T=25°C; P=11251.1 Torr; 6 h; Schlenk techniqueInert atmosphereDarkness; 2: 3,4,5-trimethoxyphenylboronic acid With potassium carbonate in dichloromethane; water T=110°C; Suzuki-Miyaura Coupling; 24 h;
参考文献
Friederici, Mario; Angurell, Inmaculada; Rossell, Oriol; Seco, Miquel; Muller, Guillermo
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 376, p. 7 - 12
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile P=7500.6 Torr; Heating; Yields of byproduct given;
参考文献
Ruemper, Joerg; Sokolov, Viktor V.; Rauch, Rarsten; De Meijere, Armin
Chemische Berichte, 1997 , vol. 130, # 9 p. 1193 - 1195
反应条件
di-tert-butyl peroxide T=140°C; P=30400 - 34200 Torr; 4 h; autoclave; Further byproducts given;
参考文献
Safiev, O. G.; Zorin, V. V.; Imashev, U. B.; Zlotskii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1388 - 1392
反应条件
aluminium trichloride-diethyl ether (1/1) T=30°C; P=1520 Torr; 0.5 h; Further byproducts given;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 54, # 5 p. 1145 - 1147,936 - 938
反应条件
aluminum tri-bromide; water T=17°C; P=1838.8 Torr;
参考文献
Socony-Vacuum Oil Co.
Patent: US2401925 , 1941 ;
反应条件
aluminium trichloride-diethyl ether (1/1) T=30°C; P=1520 Torr; 0.5 h; Further byproducts given;
参考文献
Glozshtein, A. Ya.; Sidorov, V. A.; Polyakov, S. A.; Gladysheva, T. V.
J. Appl. Chem. USSR (Engl. Transl.), 1981 , vol. 54, # 5 p. 1145 - 1147,936 - 938
反应条件
aluminium trichloride-diethyl ether (1/1) T=30°C; P=1520 Torr; 0.5 h; Further byproducts given;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 54, # 5 p. 1145 - 1147,936 - 938
反应条件
aluminium trichloride-diethyl ether (1/1) T=30°C; P=1520 Torr; 0.5 h; Further byproducts given;
参考文献
Glozshtein, A. Ya.; Sidorov, V. A.; Polyakov, S. A.; Gladysheva, T. V.
J. Appl. Chem. USSR (Engl. Transl.), 1981 , vol. 54, # 5 p. 1145 - 1147,936 - 938
反应条件
aluminium trichloride-diethyl ether (1/1) T=30°C; P=1520 Torr; 0.5 h; Further byproducts given;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 54, # 5 p. 1145 - 1147,936 - 938
反应条件
T=510°C; P=231685 Torr;
参考文献
Phillips Petr. Co.
Patent: US2209450 , 1936 ;
Full Text Show Details
Frey; Hepp
Industrial and Engineering Chemistry, 1936 , vol. 28, p. 1441ff.
