54509-73-8合成路线 （共 3623 条）
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
反应条件
sodium carbonate; K2[Ni(CN)4] T=150°C; P=125036 Torr;
参考文献
Reppe; Magin
Patent: US2577208 , 1950 ;
反应条件
methanesulfonic acid; Pd(OAc)2*1,2-bis(di-s-butylphosphino)ethane T=120°C; Product distribution; Further Variations:ratio Pd(OAc)2:ligand:CH3SO3H;
参考文献
Pugh, Robert I.; Drent, Eite
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 8 p. 837 - 840
反应条件
Pd(MeCN)2(O3STol)2; bis(1,1-diphenylphosphino)methane T=115°C; P=33752.7 Torr; 0.25 h; copolymerization; var. reactants; other temp., pressure and reaction time; Product distribution;
参考文献
Drent, E.; Broekhoven, J.A.M. van; Doyle, M.J.
Journal of Organometallic Chemistry, 1991 , vol. 417, # 1/2 p. 235 - 251
参考文献
Wickard
Patent: US2349232 , 1941 ;
参考文献
Kawamoto,K. et al.
Bulletin of the Chemical Society of Japan, 1971 , vol. 44, p. 1239 - 1243
反应条件
hydrogenchloride; dibenzoyl peroxide T=100°C; P=294203 - 367754 Torr;
参考文献
du Pont de Nemours and Co.
Patent: US2440801 , 1942 ;
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2418832 , 1942 ;
Full Text Show Details
Ford et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4323
反应条件
1: 2-Fluoro-benzoic Acid With thionyl chloride in benzene Heating / reflux; 2: ethene With AlCl3, aluminium chloride in 1,2-dichloro-ethane T=10 - 20°C;
参考文献
Allergan, Inc.
Patent: US2008/255239 A1, 2008 ;
Location in patent: Page/Page column 22; 23 ;
US 20080255239 A1
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=20°C;
参考文献
Nguyen, Phong; Corpuz, Evelyn; Heidelbaugh, Todd M.; Chow, Ken; Garst, Michael E.
Journal of Organic Chemistry, 2003 , vol. 68, # 26 p. 10195 - 10198
反应条件
sulfur trioxide in dichloromethane 0.666667 h; Ambient temperature;
参考文献
Doklady Chemistry, , vol. 276, p. 208 - 211
Doklady Akademii Nauk SSSR, , vol. 276, p. 1139 - 1143
