54509-73-8合成路线 (共 3623 条)
反应条件
N,N-bis(diphenylphosphino)-1,2,3,4-tetrahydro-1-naphthylamine; methylaluminoxane-3 Angstroem; .LAMBDA.-(+)-tris(acetylacetonato)chromium(III) in n-heptane; cyclohexane T=40°C; P=52504.2 Torr; 0.333333 h; Product distribution; Further Variations:PressuresTemperatures;
参考文献
Shozi, Mzamo L.; Friedrich, Holger B.
South African Journal of Chemistry, 2012 , vol. 65, p. 214 - 222
反应条件
in cyclohexane T=120 - 202°C; 1 - 32 h; Conversion of starting material;
参考文献
Huntsman Petrochemical Corporation
Patent: US6750374 B2, 2004 ;
Location in patent: Page column 7 ;
反应条件
carbon monoxide; ytterbium trichloride; ethylaluminum dichloride in n-heptane T=120°C; various AlEtCl2/YbCl3 ratio, other catalysts; Product distribution;
参考文献
Keim, Wilhelm; Chen, Zhongxin; Shen, Zhiquan
Journal of the Chemical Society, Chemical Communications, 1989 , # 24 p. 1923 - 1924
反应条件
bis(1,5-cyclooctadiene)nickel (0); triethylsilyl trifluoromethanesulphonate; triethylamine; diphenylcyclohexyl phosphine in toluene T=20°C; Heck type reaction; P=760.051 Torr; 2 h;
参考文献
Matsubara, Ryosuke; Gutierrez, Alicia C.; Jamison, Timothy F.
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19020 - 19023
反应条件
tetrabutylammomium bromide; PtBr2 T=150°C; 10 h;
参考文献
Rodriguez-Zubiri, Mireia; Anguille, Stephane; Brunet, Jean-Jacques; Daran, Jean-Claude
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 379, p. 103 - 111
反应条件
rhodium trichloride 3-hydrate; iodine; tetra-n-butylphosphonium iodide; triphenylphosphine T=20 - 150°C; P=18751.9 Torr; 10 h; AutoclaveInert atmosphere; Catalytic behavior; Time;
参考文献
Rodriguez-Zubiri, Mireia; Baudequin, Christine; Bethegnies, Aurelien; Brunet, Jean-Jacques
Collection of Czechoslovak Chemical Communications, 2012 , vol. 77, # 6 p. 445 - 454
反应条件
T=270°C; P=20594.2 Torr;
参考文献
Closson et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 646
反应条件
tetra-(n-butyl)-phosphonium bromide; triphenylphosphine; PtBr2 T=150°C; 10 h; AutoclaveHigh pressureSchlenk techniqueInert atmosphere; Catalytic behavior; Pressure;
参考文献
Bethegnies, Aurelien; Dub, Pavel A.; Poli, Rinaldo
Organometallics, 2013 , vol. 32, # 6 p. 1882 - 1891
反应条件
in sodium hydroxide byproducts: H2; High Pressure; heating C2H4 or C2H4 containing gas with aq. NaOH soln. at 360°C, 46 atm., 1h;;
参考文献
Na: SVol.4, 24, page 1419 - 1421
DE560907 , ;
C. II, , p. 3621
GB355866 , ;
C. I, , p. 130
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=1551.49 Torr; 24 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110