54509-73-8合成路线 (共 3623 条)
反应条件
aluminium trichloride in dichloromethane 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 22 p. 6160 - 6163
反应条件
sodium bromide (electrolysis);
参考文献
Bresson,A. et al.
Bulletin de la Societe Chimique de France, 1970 , p. 2432 - 2439
反应条件
fluorine T=-40 - 30°C; Fluorination; 1.5 h; Title compound not separated from byproducts;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
反应条件
cobalt(III) fluoride Heating;
参考文献
Maksimov, B. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1935 - 1940
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1838 - 1842
反应条件
cobalt(III) fluoride T=130 - 150°C; other hydrocarbons; var. temperatures; also CeF4 and MnF3 as fluorinating agent; Product distribution;
参考文献
Asovich, V. S.; Kornilov, V. V.; Kostyaev, R. A.; Mel'nichenko, B. A.; Maruev, A. V.; Maksimov, B. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 8 p. 1284 - 1287
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 8 p. 1221 - 1224
反应条件
cis-lt;PtCl(SnCl3)(PPh3)2gt;-silica T=119.9°C; P=31502.5 Torr; 12 h; Yield given;
参考文献
Llorca, Jordi; Piscina, Pilar Ramirez de la; Sales, Joaquim; Homs, Narcis
Journal of the Chemical Society, Chemical Communications, 1994 , # 22 p. 2555 - 2556
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=1551.49 Torr; 24 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
反应条件
di-tert-butyl peroxide T=140°C; 2 h; steel autoclave; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074
反应条件
di-tert-butyl peroxide T=140°C; 2 h; steel autoclave; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074
反应条件
di-tert-butyl peroxide T=140°C; 2 h; steel autoclave; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074