54509-73-8合成路线 (共 3623 条)
参考文献
Brumbaugh,J.S.; Sen,A.
Journal of the American Chemical Society, 1988 , vol. 110, p. 803
反应条件
MAO; N,N-bis(1H-benzimidazol-2-ylmethyl)-N-methylamine Cr(III)Cl3 in toluene T=50°C; P=3000.24 Torr; 1 h; Product distribution; Further Variations:CatalystsPressures;
参考文献
Tomov, Atanas K.; Chirinos, Juan J.; Long, Richard J.; Gibson, Vernon C.; Elsegood, Mark R. J.
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 7704 - 7705
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane T=50°C; metathesis; P=7500.6 Torr; 2 h;
参考文献
Warwel, Siegfried; Bruese, Falk; Demes, Christoph; Kunz, Michael; Klaas, Mark Ruesch gen
Chemosphere, 2001 , vol. 43, # 1 p. 39 - 48
反应条件
(Ph2PN-(Me)(CH2)2-NPPh2)CrCl3(THF) in toluene T=80°C; P=30003 Torr; 0.5 h;
参考文献
Shaikh, Yacoob; Gurnham, Joanna; Albahily, Khalid; Gambarotta, Sandro; Korobkov, Ilia
Organometallics, 2012 , vol. 31, # 21 p. 7427 - 7433,7
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=100°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Albahily, Khalid; Gambarotta, Sandro; Duchateau, Robbert
Organometallics, 2011 , vol. 30, # 17 p. 4655 - 4664
参考文献
Colubchenko, I. T.; Galoch, P. N.; Gutyrya, V. S.; Motornyi, V. G.; Khranovskaya, V. I.
Doklady Chemistry, 1981 , vol. 261, p. 521 - 523
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 261, # 4 p. 891 - 894
反应条件
tri-ruthenium(0)dodecacarbonyl in benzene T=150°C; P=29420.3 Torr; 4 h; Yield given. Yields of byproduct given;
参考文献
Tsuji, Yasushi; Ohsumi, Tatsuya; Kondo Teruyuki; Watanabe, Yoshihisa
Journal of Organometallic Chemistry, 1986 , vol. 309, p. 333 - 344
反应条件
(.eta.6-toluene)Ni(SiCl3)2 42 h; Ambient temperature; MechanismProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 108, # 8 p. 2019 - 2023
反应条件
palladium diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; biphenyl-2-yl-di-tert-butyl-phosphane in N,N-dimethyl-formamide; toluene T=120°C; Heck Reaction; P=11251.1 Torr; 0.333333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
反应条件
in pentane (Ar); reaction of Pd complex suspended in C5H12 with C2H4 (-30°C), filtration, addn. of soln. of phosphine (2 equivalents in C5H12, -78°C), crystn., evapn. to dryness (-78°C, high vacuum); not purified, 90percent pure (NMR);
参考文献
Journal of the American Chemical Society, , vol. 121, # 42 p. 9807 - 9823