54509-73-8合成路线 (共 3623 条)
参考文献
Read; Williams
Journal of the Chemical Society, 1917 , vol. 111, p. 241
参考文献
Rust; Vaughan
Journal of Organic Chemistry, 1942 , vol. 7, p. 495
参考文献
Read; Williams
Journal of the Chemical Society, 1917 , vol. 111, p. 241
反应条件
in n-heptane byproducts: (CH2CHCHCH2CH(CH3))x; High Pressure; (Ar); to a soln. of Al-compound added ethylene (20 bar pressure) under stirring at 100°C for 24 h; distd. in vacuo at 50°C; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
反应条件
in further solvent(s) (Ar); ethylene bubbled through a soln. of Al-compound in a mixture of hydrocarbons (C10-C14) at 150°C for 48 h; distd.; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
反应条件
in n-heptane byproducts: (CH2CHCHCH2CH(CH3))x; High Pressure; (Ar); to a soln. of Al-compound and Al added ethylene (20 bar pressure) under stirring at 100-150°C for 16 h; distd. in vacuo at 50°C; elem. anal.;
参考文献
Martin, Heinz; Bretinger, Helmut
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 2 p. 182 - 186
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium; [(t-Bu3P)PdBr]2 in tetrahydrofuran T=60°C; P=7500.75 Torr; 16 h; Autoclave;
参考文献
Baader, Sabrina; Ohlmann, Dominik M.; Goossen, Lukas J.
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9807 - 9810
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
反应条件
(i) LiAlH4, TiCl4, THF, (ii) /BRN= 605309/, CuCl; Multistep reaction;
参考文献
Sato,F. et al.
Chemistry Letters, 1978 , p. 805 - 806
反应条件
carbon in gaseous matrix Irradiation; Mechanism;
参考文献
Kaiser; Lee; Suits
Journal of Chemical Physics, 1996 , vol. 105, # 19 p. 8705 - 8720