54509-73-8 合成路线 （共 3623 条）
反应条件
ethylbis(triphenylphosphine)nickel chloride in benzene T=20°C; other nickel complexes; Product distribution;
参考文献
Furman, D. B.; Volchkov, N. V.; Isaeva, L. S.; Morozova, L. N.; Kravtsov, D. N.; Bragin, O. V.
反应条件
(triphenylphosphine)3(CO)nickelk in n-heptane T=20°C; 0.5 h; other solvents; Product distribution;
参考文献
Furman, D. B.; Volchkov, N. V.; Makhlis, L. A.; Matkovskii, P. E.; Belov, G. P.; et al.
反应条件
1: in toluene T=20 - 116°C; P=26252.6 - 42004.2 Torr; 2.33333 h; 2: With sulfuric acid; water T=40°C;
参考文献
WO2005/123639 A1, ;
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反应条件
17741-60-5 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-二十一氟十二烷醇丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
water; sodium carbonate in dichloromethane 1 h; Ambient temperature;
参考文献
Umemoto, Teruo; Kuriu, Yuriko; Nakayama, Shin-ichi
参考文献
Brintzinger; Langheck
反应条件
1: ethene With bis(1,5-cyclooctadiene)nickel (0); dtbpe in chlorobenzene T=45°C; P=15001.5 Torr; 0.5 h; Autoclave; 2: carbon dioxide in chlorobenzene T=20 - 60°C; P=7500.75 - 37503.8 Torr; 3: With sodium t-butanolate in chlorobenzene 1 h;
参考文献
BASF SE; BASF (CHINA) COMPANY LIMITED; LIMBACH, Michael; LINDNER, Ronald; LEJKOWSKI, Michael Ludwik; KAGEYAMA, Takeharu; BODIZS, Gabriella Eva; SCHUNK, Stephan; FUTTER, Cornelia; ROTHER, Jörg
反应条件
in tetrahydrofuran P=22502.3 Torr; 18 h; Inert atmosphere;
参考文献
Lejkowski, Michael L.; Lindner, Ronald; Kageyama, Takeharu; Bodizs, Gabriella E.; Plessow, Philipp N.; Mueller, Imke B.; Schaefer, Ansgar; Rominger, Frank; Hofmann, Peter; Futter, Cornelia; Schunk, Stephan A.; Limbach, Michael
