54509-73-8合成路线 (共 3623 条)
反应条件
triphenylphosphine in not given byproducts: CH2CHSiMe3; react. of Ru-complex with ethylene (50 kg cm**-2) at 70°C in the presence of an equimolar amt. of PPh3;
参考文献
Wakatsuki, Yasuo; Yamazaki, Hiroshi; Nakano, Masato; Yamamoto, Yasuhiro
Journal of the Chemical Society, Chemical Communications, 1991 , # 10 p. 703 - 704
反应条件
di-tert-butyl peroxide T=150°C; P=51485.6 Torr;
反应条件
water; hydrogen T=80 - 95°C; Einwirkung von stillen elektrischen Entladungen;
参考文献
Shell Devel.Co.
Patent: US2672440 , 1951 ;
反应条件
water; molecular sieve T=350°C; 1 h; var. aluminophosphate based molecular sieves containing Ni and Zn, temp., reaction times, and partial pressures of water; Product distribution;
参考文献
Kannan; Elangovan; Palanichamy; Murugesan
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1998 , vol. 37, # 7 p. 655 - 658
参考文献
Justus Liebigs Annalen der Chemie, , vol. 561, p. 101
X. Congr.int.Chim. Rom 1938 Bd.4 S. 279 C.A. 1940 3237
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 206, p. 1663
Chem.Abstr., , p. 3237
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=562.556 Torr; 24 h; Inert atmosphere;
参考文献
WO2011/2284 A1, ;
Page/Page column 19 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=562.556 Torr; 24 h; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2011/2284 A1, ;
Page/Page column 19 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=375.038 Torr; 48 h; Inert atmosphereGreen chemistry; Reagent/catalystPressureConcentration;
参考文献
Green Chemistry, , vol. 14, # 10 p. 2747 - 2751,5
反应条件
Grubbs Ruthenium metathesis catalyst T=0 - 50°C; 24 h;
参考文献
WO2009/45637 A2, ;
Page/Page column 42; 1/4; 3/4 ;