54509-73-8合成路线 (共 3623 条)
参考文献
Oehman
Chem.Abstr., 1945 , p. 1113
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Oehman
Svedberg-Festschrift <Uppsala 1944> S. 416
反应条件
iron(III) chloride T=60 - 100°C;
参考文献
Asscher,M.; Vofsi,D.
Journal of the Chemical Society, 1964 , p. 4962 - 4971
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=70°C; Mizoroki-Heck reaction; 24 h;
参考文献
Hirabayashi, Kazunori; Ando, Jun-Ichi; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 6 p. 1409 - 1417
反应条件
C5H2Ph4; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper diacetate in 1,2-dichloro-ethane T=120°C; P=3750.38 Torr; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Shi, Zhuangzhi; Schroeder, Nils; Glorius, Frank
Angewandte Chemie - International Edition, 2012 , vol. 51, # 32 p. 8092 - 8096
反应条件
neopentane2,2-dimethylpropane in dichloromethane T=14 - 15°C; 4 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tlumak, Robert L.; Day, James C.; Slanga, Joseph P.; Skell, Philip S.
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7257 - 7267
反应条件
di-tert-butyl peroxide T=140°C; 2 h; steel autoclave; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074
反应条件
di-tert-butyl peroxide T=140°C; 2 h; steel autoclave; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074
反应条件
di-tert-butyl peroxide T=140°C; 2 h; various molar ratios; Product distribution;
参考文献
Germash, A. V.; Zorin, V. V.; Nikolaeva, S. V.; Zlot-skii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 10 p. 2328 - 2332,2071 - 2074
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Germash, A. V.; Dostovalova, V. I.; Zorin, V. V.; Terent'ev, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 1 p. 173 - 178
反应条件
pentacarbonyliron(0); water T=120 - 125°C; P=139746 - 147102 Torr;
参考文献
BASF
Patent: DE839800 , 1943 ;
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Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
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Reppe,W.
Acetylene Chemistry <New York 1949> S.180