54509-73-8合成路线 （共 3623 条）
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 173 - 178
反应条件
aluminium trichloride in dichloromethane T=-10°C; 0.25 h;
参考文献
Ellingboe, John W.; Lombardo, Louis J.; Alessi, Thomas R.; Nguyen, Thomas T.; Guzzo, Frieda; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 17 p. 2485 - 2493
参考文献
Pelter,A. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 145 - 150
反应条件
aluminium trichloride T=0°C;
参考文献
Cheung, Adrian Wai-Hing; Danho, Waleed; Swistok, Joseph; Qi, Lida; Kurylko, Grazyna; Rowan, Karen; Yeon, Mitch; Franco, Lucia; Chu, Xin-Jie; Chen, Li; Yagaloff, Keith
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 133 - 137
反应条件
silica gel T=350 - 360°C;
参考文献
Sharples Chem. Inc.
Patent: US2422632 , 1944 ;
Full Text Show Details
Sharples Chem. Inc
Chem.Abstr., 1947 , p. 5892
反应条件
T=275 - 375°C; ueber Dehydratisierungs- und Hydrierungs-Katalysatoren unter Druck;
参考文献
Sharples Chem.Inc.
Patent: US2422632 , 1944 ;
Full Text Show Details
Sharples Chem.Inc.
Patent: US2422631 , 1944 ;
反应条件
T=275 - 375°C; ueber Dehydratisierungs- und Hydrierungs-Katalysatoren unter Druck;
参考文献
Sharples Chem.Inc.
Patent: US2422632 , 1944 ;
Full Text Show Details
Sharples Chem.Inc.
Patent: US2422631 , 1944 ;
反应条件
sodium tetrahydroborate in ethanol heated at 60°C and 40 bar in autoclave for 4 h; filtered, washed (H2O, EtOH, pentane), elem. anal.;
参考文献
Chemische Berichte, , vol. 115, # 5 p. 1998 - 1999
反应条件
in ethanol bubbling ethene into stirred soln. of Pt-complex in EtOH to saturation (under N2), slow addn. of B-compd., bubbling ethene (2 h); filtration, washing (H2O, EtOH), drying in air;
参考文献
Journal of Organometallic Chemistry, , vol. 388, # 1+2 p. 215 - 220
反应条件
in ethanol dissolution of Pt-compd. in EtOH, satn. with ethylene, addn. of soln. of NaBH4 in EtOH (ethylene flow); filtration, washing (EtOH), drying;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 23, p. 251 - 252
