54509-73-8合成路线 （共 3623 条）
反应条件
T=253°C; P=38000 Torr; mit Phosphaten der Gruppe III;Prod.5-7:Diaethylaether,Propylisopropylaether,Aethylalkohol;
参考文献
Newitt; Semerano
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1936 , vol. 157, p. 354
反应条件
MAO; N,N-bis(1H-benzimidazol-2-ylmethyl)-N-methylamine Cr(III)Cl3 in toluene T=50°C; P=3000.24 Torr; 1 h; Product distribution; Further Variations:CatalystsPressures;
参考文献
Tomov, Atanas K.; Chirinos, Juan J.; Long, Richard J.; Gibson, Vernon C.; Elsegood, Mark R. J.
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 7704 - 7705
反应条件
tetrafluoroboric acid; water; mercury(II) oxide 1.) THF, -10 deg C, 5 min, 2.) reflux, 6 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 376 - 378
反应条件
hydrogen T=80°C; P=15001.5 Torr; 70 h; Inert atmosphereFlow reactor; Catalytic behavior; Reagent/catalyst; regioselective reaction;
参考文献
Schoenweiz, Andreas; Debuschewitz, Jonas; Walter, Simon; Woelfel, Rene; Hahn, Hanna; Dyballa, Katrin M.; Franke, Robert; Haumann, Marco; Wasserscheid, Peter
ChemCatChem, 2013 , vol. 5, # 10 p. 2955 - 2963
反应条件
AlCl3, aluminium chloride in dichloromethane T=0 - 5°C; Friedel Crafts Alkylation;
参考文献
MERCK and CO., INC.
Patent: WO2007/61694 A2, 2007 ;
Location in patent: Page/Page column 51; 71-72 ;
WO 2007/061694 A2
反应条件
1: 2-(3-Bromo-phenyl)-acetic acid With oxalyl dichloride T=20°C; 5.08333 h; Heating / reflux; 2: ethene With AlCl3, aluminium chloride in dichloromethane T=0 - 5°C; Friedel Crafts reaction;
参考文献
MERCK and CO. INC.
Patent: WO2004/83187 A1, 2004 ;
Location in patent: Page 39-40 ;
WO 2004/083187 A1
反应条件
aluminium trichloride T=0°C;
参考文献
Cheung, Adrian Wai-Hing; Danho, Waleed; Swistok, Joseph; Qi, Lida; Kurylko, Grazyna; Rowan, Karen; Yeon, Mitch; Franco, Lucia; Chu, Xin-Jie; Chen, Li; Yagaloff, Keith
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 1 p. 133 - 137
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 26, p. 1405 - 1413
反应条件
sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=130°C; P=760 Torr; 8 h;
参考文献
Spencer, Alwyn
Journal of Organometallic Chemistry, 1983 , vol. 258, # 1 p. 101 - 108
反应条件
sodium carbonate; K2[Ni(CN)4] T=150°C; P=95616 - 110326 Torr;
参考文献
Reppe; Magin
Patent: US2577208 , 1950 ;
