54509-73-8合成路线 (共 3623 条)
反应条件
{[P(cyclohexyl)3]2RuCl(CO)(3-methylbut-2-enylidene)}BF4 in benzene T=80°C; 48 h;
参考文献
Yi, Chae S.; Sang, Young Yun
Organic Letters, 2005 , vol. 7, # 11 p. 2181 - 2183
反应条件
sodium; copper(II) oxide T=300°C; P=147102 Torr;
参考文献
Stroh et al.
Angewandte Chemie, 1957 , vol. 69, p. 124,126
反应条件
di-tert-butyl peroxide T=140°C; P=30400 - 34200 Torr; 4 h; autoclave; Further byproducts given;
参考文献
Safiev, O. G.; Zorin, V. V.; Imashev, U. B.; Zlotskii, S. S.; Terent'ev, A. B.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1192 - 1195
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1388 - 1392
反应条件
di-tert-butyl peroxide
参考文献
Safiev,O.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 2313 - 2316
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, p. 2499 - 2502
反应条件
1: in toluene T=20 - 116°C; P=26252.6 - 42004.2 Torr; 2.33333 h; 2: With sulfuric acid; water T=40°C;
参考文献
WO2005/123639 A1, ;
Page/Page column 10-11 ;
反应条件
1: in toluene T=20 - 116°C; P=17851.8 - 42004.2 Torr; 2 - 3 h; 2: With sulfuric acid; water T=40°C; Product distribution / selectivity;
参考文献
WO2005/123639 A1, ;
Page/Page column 8-9 ;
反应条件
cobalt + iron; water; hydrogen T=110 - 178°C; P=404529 - 536921 Torr;
参考文献
du Pont de Nemours and Co.
Patent: US2437600 , 1945 ;
反应条件
hydrogen; silica gel; rhodium T=180°C; 1.5 h; oxo selectivity; variation of particle size of Rh catalyst; Product distribution;
参考文献
Arakawa, Hironori; Takahashi, Nobuo; Hanaoka, Takaaki; Takeuchi, Kazuhiko; Matsuzaki, Takehiko; Sugi, Yoshihiro
Chemistry Letters, 1988 , p. 1917 - 1918
反应条件
tris(triphenylphosphine)ruthenium(II) chloride T=210°C; 18 h; other aldehydes and olefines; Product distribution;
参考文献
Isnard, P.; Denise, B.; Sneeden, R. P. A; Cognion, J. M.; Durual, P.
Journal of Organometallic Chemistry, 1982 , vol. 240, # 3 p. 285 - 288
反应条件
[Rh(acac)2(CO)2]; hydrogen; silica gel; diethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene P=7500.75 Torr; 20 h; Catalytic behavior; Reagent/catalyst;
参考文献
Schneider, Martin Johannes; Lijewski, Martin; Woelfel, Rene; Haumann, Marco; Wasserscheid, Peter
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6996 - 6999
Angew. Chem., 2013 , vol. 127, # 27 p. 7134 - 7137,4