54509-73-8合成路线 （共 3623 条）
反应条件
isovaleric acid methyl ester; di-tert-butyl peroxide T=140°C; P=30400 - 38000 Torr; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Terent'ev, A. B.; Dostovalova, V. I.; Ikonnikov, N. S.; Moskalenko, M. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 377 - 382
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 558 - 563
反应条件
sodium carbonate; triethylamine; palladium dichloride; Tl(OCOCF3)3 Yield given. Multistep reaction;
参考文献
Larock, R. C.; Varaprath, S.; Lau, H. H.; Fellows, C. A.
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5274 - 5284
反应条件
sodium carbonate; triethylamine; lithium chloride; palladium dichloride; Tl(OCOCF3)3 relative product ratio; Product distribution;
参考文献
Larock, R. C.; Varaprath, S.; Lau, H. H.; Fellows, C. A.
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5274 - 5284
反应条件
copper diacetate; manganese triacetate in acetic acid; ethyl acetate P=76000.1 Torr; 4 h; var. conc. of reagents, var. pressure; Product distributionMechanism;
参考文献
Vinogradov, M. G.; Petrenko, O. N.; Verenchikov, S. P.; Nikishin, G. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 4 p. 626 - 631
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 4 p. 714 - 720
反应条件
tetrachloromethane T=-15°C;
参考文献
Boehme et al.
Justus Liebigs Annalen der Chemie, 1957 , vol. 602, p. 1,13
反应条件
tetrachloromethane T=40 - 50°C;
参考文献
Boehme; Clement
Justus Liebigs Annalen der Chemie, 1952 , vol. 576, p. 61,67
反应条件
AlCl3, aluminium chloride Friedel Crafts alkylation;
参考文献
Schuisky, Peter; Federsel, Hans-Juergen; Tian, Wei
Journal of Organic Chemistry, 2012 , vol. 77, # 13 p. 5503 - 5514
反应条件
aluminium trichloride in dichloromethane T=-15°C; Cycloaddition; 1.5 h;
参考文献
Yao; Pollack
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 634 - 638
反应条件
(i), (ii) MeMgHal; Multistep reaction;
参考文献
Freidlina,R.Kh. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1961 , p. 1168 - 1171
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , # 7 p. 1256 - 1261
反应条件
1: para-xylene With n-butyllithium; LiK(OCH2CH2NMe2)2; Mg(OCH2CH2OEt)2 in various solvent(s) T=20°C; Metallation; 0.5 h; 2: ethene in various solvent(s) T=80°C; Alkylation; P=7600.51 Torr; 24 h; Further stages.;
参考文献
Steele, Barry R.; Screttas, Constantinos G.
Journal of the American Chemical Society, 2000 , vol. 122, # 10 p. 2391 - 2392
