54509-73-8合成路线 （共 3623 条）
反应条件
Grubb's 2nd generation catalyst in toluene T=60°C; P=12929 - 15514.9 Torr; 1.5 h; Inert atmosphere;
参考文献
AMYRIS, INC.; SCHOFER, Susan; SAFIR, Adam; VAZQUEZ, Roberto
Patent: WO2013/82264 A1, 2013 ;
Location in patent: Paragraph 00168 ;
反应条件
Hoveyda-Grubbs second generation catalyst in toluene T=30°C; P=7500.75 Torr; Inert atmosphere; TemperaturePressureReagent/catalyst;
参考文献
AMYRIS, INC.; SCHOFER, Susan; SAFIR, Adam; VAZQUEZ, Roberto
Patent: WO2013/82264 A1, 2013 ;
Location in patent: Paragraph 00169-00178 ;
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=3750.38 Torr; 24 h; Inert atmosphereGreen chemistry; PressureConcentration;
参考文献
Spekreijse, Jurjen; Le Notre, Jerome; Scott, Elinor L.; Sanders, Johan P. M.; Van Haveren, Jacco
Green Chemistry, 2012 , vol. 14, # 10 p. 2747 - 2751,5
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; P=750.075 Torr; 24 h; Inert atmosphereGreen chemistry; PressureConcentration;
参考文献
Spekreijse, Jurjen; Le Notre, Jerome; Scott, Elinor L.; Sanders, Johan P. M.; Van Haveren, Jacco
Green Chemistry, 2012 , vol. 14, # 10 p. 2747 - 2751,5
反应条件
T=150°C; P=22065.2 Torr;
参考文献
Pines; Wunderlich
Journal of the American Chemical Society, 1959 , vol. 81, p. 2568,2569
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 173 - 178
反应条件
(i) SO2Cl2, AlCl3, (ii) aq. Cl2; Multistep reaction;
参考文献
Titov,A.I.; Baryshnikova,A.N.
Doklady Chemistry, 1964 , vol. 157, # 1 p. 681 - 684
Doklady Akademii Nauk SSSR, 1964 , vol. 157, # 1 p. 139 - 142
反应条件
lt;Ti(OC6H3Ph2-2,6)2(C12H20)gt;
参考文献
Journal of the American Chemical Society, , vol. 119, # 33 p. 7685 - 7693
反应条件
(Ph2PN-(Me)(CH2)2-NPPh2)CrCl3(THF) in toluene T=80°C; P=30003 Torr; 0.5 h;
参考文献
Organometallics, , vol. 31, # 21 p. 7427 - 7433,7
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
Full Text Show Details
Shelton; Lee
Journal of Organic Chemistry, 1958 , vol. 23, p. 1876,1880
