54509-73-8合成路线 (共 3623 条)
反应条件
methylalumoxane (PMAO-S) in toluene T=80°C; P=15001.5 Torr; 1 h; Product distribution / selectivity;
参考文献
Braunstein, Pierre; Chauvin, Yves; Mercier, Sophie; Saussine, Lucien; Cian, Andre De; Fischer, Jean
Journal of the Chemical Society, Chemical Communications, 1994 , # 19 p. 2203 - 2204
反应条件
1: With tri(n-octyl)aluminium in toluene T=80°C; 2: With CrCl3(THF)3; bis(di{ortho-methoxyphenyl}phosphanyl)(methyl)amine in toluene T=80°C; 1 h; Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2006/293546 A1, 2006 ;
Location in patent: Page/Page column 7-8 ;
反应条件
(Ph2PN-(Me)(CH2)2-NPPh2)CrCl3(THF) in toluene T=80°C; P=30003 Torr; 0.5 h;
参考文献
Shaikh, Yacoob; Gurnham, Joanna; Albahily, Khalid; Gambarotta, Sandro; Korobkov, Ilia
Organometallics, 2012 , vol. 31, # 21 p. 7427 - 7433,7
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=100°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Albahily, Khalid; Gambarotta, Sandro; Duchateau, Robbert
Organometallics, 2011 , vol. 30, # 17 p. 4655 - 4664
反应条件
hydrogenchloride; (1,5,9-cyclododecatrien)Ni(I); dcype 1.) toluene, RT, 7 d, 2.) toluene, 1 bar; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 3 p. C51 - C53
反应条件
(1,5,9-cyclododecatrien)Ni(I); dcype multistep reaction; var. reaction products depending on second-step reaction partner; other ligand; other alkenes; var. temperatures and time;
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 3 p. C51 - C53
反应条件
(i) Cl2, (ii) H2O, (iii) NaOH, diethylene glycol; Multistep reaction;
参考文献
Beger,J. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 408 - 419
反应条件
hydrogenchloride in methanol T=5 - 10°C; P=45003.6 Torr; electrolysis, further solvent aq. acetonitrile;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 523 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 582 - 584
反应条件
chlorine in der Gasphase;
参考文献
Buss, E.; Rockstuhl, A.; Schnurpfeil, D.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 2 p. 197 - 208
反应条件
hydrogenchloride T=5 - 10°C; P=45003.6 Torr; electrolysis;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 3 p. 523 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 582 - 584