54509-73-8合成路线 （共 3623 条）
反应条件
1: With zirconocene dichloride; ethylaluminum dichloride; magnesium in tetrahydrofuran 6 h; Inert atmosphere; 2: With sulfur in benzene T=80°C; 6 h; Inert atmosphere;
参考文献
Ibragimov; Khafizova; Khusainova; Tyumkina; Dzhemilev
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 4 p. 474 - 479
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Xi, Zhenfeng; Hara, Ryuichiro; Takahashi, Tamotsu
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4444 - 4448
反应条件
sulfuric acid in acetic acid Irradiation;
参考文献
Neale,R.S.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3263 - 3273
反应条件
(i) Cl2, (ii) H2S, (iii) aq. NaOH; Multistep reaction;
参考文献
Beger,J. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 408 - 419
反应条件
(i) AlCl3, CS2, (ii) /BRN= 1730731/; Multistep reaction;
参考文献
Baisted,D.J.; Whitehurst,J.S.
Journal of the Chemical Society, 1965 , p. 2340 - 2349
反应条件
(i) SO2Cl2, CCl4, (ii) /BRN= 1730731/, CH2Cl2, (iii) KOH, EtOH; Multistep reaction;
参考文献
McClelland,R.A.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 548 - 551
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile P=7500.6 Torr; Heating; Yields of byproduct given;
参考文献
Ruemper, Joerg; Sokolov, Viktor V.; Rauch, Rarsten; De Meijere, Armin
Chemische Berichte, 1997 , vol. 130, # 9 p. 1193 - 1195
反应条件
aluminium trichloride in benzene T=100°C; P=15514.4 Torr;
参考文献
Allen,C.F.H. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 778 - 779
反应条件
aluminium trichloride; pentane T=-20°C; Kochen der neben 1-Brom-3.3-dimethyl-pentan entstehenden Verbindung C9H19Br mit Zink und Isopropylalkohol;
参考文献
Universal Oil Prod.Co.
Patent: US2434289 , 1944 ;
反应条件
silver tetrafluoroborate; Br(1-)*C29H31BrN5Pt(1+) in PhNO2-d5 T=20 - 150°C; P=4125.41 Torr; 26 h; Inert atmosphere;
参考文献
Cao, Peng; Cabrera, Jose; Padilla, Robin; Serra, Daniel; Rominger, Frank; Limbach, Michael
Organometallics, 2012 , vol. 31, # 3 p. 921 - 929
