54509-73-8合成路线 (共 3623 条)
反应条件
silica gel; ruthenium T=49.9°C; other alkenes, other catalyst; Mechanism;
参考文献
Koerts, Tijs; Santen, Rutger A. van
Journal of the Chemical Society, Chemical Communications, 1992 , # 4 p. 345 - 346
反应条件
tantalum pentafluoride P=1034.3 - 3102.9 Torr; 0.333333 h; Ambient temperatureother reagents (solid superacids); Product distribution;
参考文献
Olah, George A.; Felberg, Jeff D.; Lammertsma, Koop
Journal of the American Chemical Society, 1983 , vol. 105, # 21 p. 6529 - 6531
反应条件
potassium chloride in hydrogenchloride dissoln. of Pt-complex in concd. HCl, addn. of H2O, bubbling ethene through soln. for 5 d at room temp.; evapn., extn. into 4percent HCl in EtOH, filtration off of KCl, evapn. (reduced pressure), washing (Et2O), extn. into CHCl3, evapn., recrystn. (CH2Cl2/Et2O=1:1, -35°C); elem. anal.;
参考文献
Plutino, Maria Rosaria; Otto, Stefanus; Roodt, Andreas; Elding, Lars I.
Inorganic Chemistry, 1999 , vol. 38, # 6 p. 1233 - 1238
反应条件
catalyst: butylene in not given
参考文献
Chernyaev, I. I.; Gel'man, A. D.
Izv. Plat., 1937 , vol. 14, p. 77 - 121
Full Text Show Details
Gmelin Handbook: Pt: MVol.D, 194, page 428 - 431
反应条件
hydrogenchloride in hydrogenchloride byproducts: KCl; passing N2 foe 10 min through soln. of PtCl4(2-) (prepd. from PtCl6(2-)and N2H4*HCl), addn. of concd. HCl to give 1 M HCl, stirring under 100 psi C2H4 for 48 h; removal of volatiles (vac.), extn. into EtOH, filtration, solvent removal (vac.);
参考文献
Boag, Neil M.; Ravetz, Megan S.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 21 p. 3473 - 3474
反应条件
in hydrogenchloride treatment of a HCl-containing H2(PtCl4)-soln. with ethylene for several days under pressure; treatment with solid KCl;;
参考文献
Gmelin Handbook: Pt: MVol.D, 194, page 428 - 431
参考文献
Tartakovskii,V.A. et al.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 232 - 235
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, p. 240 - 243
反应条件
phosphorus-modified zeolite-ZSM-5 T=320°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Mravec, Dusan; Herain, Jiri; Holotik, Stefan
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, # 8 p. 1832 - 1839
参考文献
Bondarenko et al.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1957 , vol. 30, p. 781; engl. Ausg. S. 822
反应条件
bromine; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 48 h; Heating;
参考文献
Katayama, Hiroyuki; Fukuse, Yosuke; Nobuto, Yuko; Akamatsu, Kensuke; Ozawa, Fumiyuki
Macromolecules, 2003 , vol. 36, # 19 p. 7020 - 7026