54509-73-8合成路线 (共 3623 条)
反应条件
(i) SO2Cl2, CCl4, (ii) /BRN= 1730731/, CH2Cl2, (iii) KOH, EtOH; Multistep reaction;
参考文献
McClelland,R.A.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 548 - 551
反应条件
C39H57MoN2PSi2 T=50°C; 15 h; Inert atmosphere;
参考文献
Khalimon, Andrey Y.; Simionescu, Razvan; Nikonov, Georgii I.
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 7033 - 7053
反应条件
C21H34FeO2Si4 in toluene T=20°C; P=760.051 Torr; 5 h; Schlenk technique;
参考文献
Sunada, Yusuke; Tsutsumi, Hironori; Shigeta, Keisuke; Yoshida, Ryota; Hashimoto, Toru; Nagashima, Hideo
Dalton Transactions, 2013 , vol. 42, # 48 p. 16687 - 16692
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Germash, A. V.; Dostovalova, V. I.; Zorin, V. V.; Terent'ev, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 1 p. 173 - 178
反应条件
bis(cyclopentadienyl)titanium dichloride; tert.-butyl lithium in tetrahydrofuran; pentane T=25°C; 2 h;
参考文献
Tsubouchi, Akira; Nishio, Emi; Kato, Yoshiko; Fujiwara, Tooru; Takeda, Takeshi
Tetrahedron Letters, 2002 , vol. 43, # 33 p. 5755 - 5758
反应条件
4 A molecular sieve; magnesium; triethyl phosphite; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran 0.5 h; Heating;
参考文献
Tsubouchi, Akira; Nishio, Emi; Kato, Yoshiko; Fujiwara, Tooru; Takeda, Takeshi
Tetrahedron Letters, 2002 , vol. 43, # 33 p. 5755 - 5758
反应条件
1: With C29H31Cl3CrNO4P2 in chlorobenzene T=20°C; P=760.051 Torr; 2: With 10 palladium on activated charcoal; hydrogen in chlorobenzene Inert atmosphere;
参考文献
Do, Loi H.; Labinger, Jay A.; Bercaw, John E.
Organometallics, 2012 , vol. 31, # 14 p. 5143 - 5149
反应条件
boron trifluoride diethyl etherate
参考文献
Farbw. Hoechst
Patent: DE926965 , 1952 ;
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Izumi, Taeko; Nishimoto, Yasuhiro; Kohei, Kunihiro; Kasahara, Akira
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1419 - 1424
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate in methanol T=60°C; P=3750.38 Torr; 16 h; Autoclave;
参考文献
Rakshit, Souvik; Grohmann, Christoph; Besset, Tatiana; Glorius, Frank
Journal of the American Chemical Society, 2011 , vol. 133, # 8 p. 2350 - 2353