54509-73-8合成路线 （共 3623 条）
反应条件
T=320 - 340°C; P=147102 Torr;
参考文献
Stroh et al.
Angewandte Chemie, 1957 , vol. 69, p. 699,700
反应条件
acetophenone in acetonitrile 5 h; Irradiation;
参考文献
Faure, Sophie; Jensen, Anders A.; Maurat, Vincent; Gu, Xin; Sagot, Emmanuelle; Aitken, David J.; Bolte, Jean; Gefflaut, Thierry; Bunch, Lennart
Journal of Medicinal Chemistry, 2006 , vol. 49, # 22 p. 6532 - 6538
反应条件
AlCl3, aluminium chloride in dichloromethane T=-10 - 0°C;
参考文献
THE WELLCOME FOUNDATION LIMITED
Patent: EP1199307 A1, 2002 ;
Location in patent: Page 12 ;
反应条件
aluminium chloride in dichloromethane
参考文献
Burroughs Wellcome Co.
Patent: US5405851 A1, 1995 ;
US 5405851 A
反应条件
aluminium trichloride; N,N-dimethyl-formamide 1.) CH2Cl2, 20-25 deg C, 18 h, 2.) 0-5 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Tschaen, David M.; Abramson, Lee; Cai, Dongwei; Desmond, Richard; Dolling, Ulf-H.; et al.
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4324 - 4330
反应条件
aluminium trichloride T=5 - 10°C;
参考文献
Roehm and Haas Co.
Patent: US2004046 , 1931 ;
反应条件
aluminium trichloride T=0°C;
参考文献
Spring; Vickerstaff
Journal of the Chemical Society, 1935 , p. 1873
参考文献
Roehm and Haas Co.
Patent: US2004069 , 1931 ;
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h; Reagent/catalystSolventTemperature;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
参考文献
Uschakow; Tschistow; Schlossberg
Zhurnal Obshchei Khimii, 1935 , vol. 5, p. 1397
Chem. Zentralbl., 1937 , vol. 108, # I p. 3619
