54509-73-8合成路线 （共 3623 条）
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) in ethanol T=110°C; P=37503 Torr; 2 h;
参考文献
Jones, M. D.
Journal of Organometallic Chemistry, 1989 , vol. 366, p. 403 - 408
反应条件
Mo(NC6H3(CH(CH3)2)2)(CHC(CH3)2C6H5)(NC4H2(CH3)2)(OC10H9BrC10H9BrOSi(CH3)2C(CH3)3) in 1,3,5-trimethyl-benzene P=7600.51 Torr; 16 h; Inert atmosphereSealed system; Product distribution / selectivity;
参考文献
Massachusetts Institute of Technology; Trustees of Boston College
Patent: US2011/15430 A1, 2011 ;
Location in patent: Page/Page column 12 ;
反应条件
aluminum oxide; tetramethylstannane; Re2O7 T=90°C; P=37503 Torr;
参考文献
Warwel, Siegfried; Kaetker, Hans; Rauenbusch, Claudia
Angewandte Chemie, 1987 , vol. 99, # 7 p. 714 - 715
反应条件
Re2O7/B2O3/Al2O3; tetramethylstannane in toluene P=3750.38 - 4500.45 Torr; 4.33 h; Product distribution / selectivity;
参考文献
MILTITZ AROMATICS GMBH
Patent: WO2006/89675 A1, 2006 ;
Location in patent: Page/Page column 7; 8; 9; 10; 11 ;
反应条件
Re2O7/B2O3/Al2O3; tetramethylstannane in toluene P=3750.38 - 4500.45 Torr; 31.75 h; Product distribution / selectivity;
参考文献
MILTITZ AROMATICS GMBH
Patent: WO2006/89675 A1, 2006 ;
Location in patent: Page/Page column 10; 11 ;
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in N,N-dimethyl-formamide T=110°C; Heck reaction; P=30002.4 Torr; 24 h;
参考文献
Heinenberg, Michael; Menges, Bernhard; Mittler, Silvia; Ritter, Helmut
Macromolecules, 2002 , vol. 35, # 9 p. 3448 - 3455
反应条件
1: o-toluidine With n-butyllithium; LiK(OCH2CH2NMe2)2 in various solvent(s) T=20°C; 0.5 h; 2: ethene With Mg(OCH2CH2OEt)2 in various solvent(s) T=80°C; P=7600.51 Torr; 24 h; Further stages.;
参考文献
Steele, Barry R.; Georgakopoulos, Spyros; Micha-Screttas, Maria; Screttas, Constantinos G.
European Journal of Organic Chemistry, 2007 , # 19 p. 3091 - 3094
反应条件
triethylamine; palladium diacetate; tris-(o-tolyl)phosphine T=20 - 80°C; P=9750.98 - 10501.1 Torr; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP2236504 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
carbon disulfide; aluminium trichloride T=0°C; Anschliessend Erwaermen auf 40-45grad;
参考文献
McMahon et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2976
反应条件
lt;(allyl)Pd(Ph2PCH2C(=O)OMe)gt;SbF6 in dichloromethane T=50°C; P=18751.5 Torr; 7 h; other temp.; other time; other palladium catalysts; Product distribution;
参考文献
Keim, Wilhelm; Maas, Heiko; Mecking, Stefan
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995 , vol. 50, # 3 p. 430 - 438
