54509-73-8合成路线 （共 3623 条）
反应条件
von ueberschuessigem Propionylchlorid;
参考文献
Gunstone; Heggie
Journal of the Chemical Society, 1952 , p. 1437,1441
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
反应条件
1: With C29H31Cl3CrNO4P2 in chlorobenzene T=20°C; P=760.051 Torr; 2: With 10 palladium on activated charcoal; hydrogen in chlorobenzene Inert atmosphere;
参考文献
Do, Loi H.; Labinger, Jay A.; Bercaw, John E.
Organometallics, 2012 , vol. 31, # 14 p. 5143 - 5149
反应条件
n-heptane; sodium T=200°C; P=588406 - 735508 Torr;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1899,1901
反应条件
analog reagieren wie das Butylamin;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1899,1901
反应条件
T=160°C; P=110326 Torr;
参考文献
Degussa
Patent: US2768196 , 1954 ;
Full Text Show Details
Degussa
Patent: US2833808 , 1957 ;
反应条件
in diethyl ether byproducts: methane; react. with 3 equiv. of ethylene at room temp. and atmospheric pressure; recrystn.;
参考文献
Wielstra, Ytsen; Gambarotta, Sandro; Chiang, Michael Y.
Organometallics, 1988 , vol. 7, p. 1866 - 1867
参考文献
Cooper,P. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 3031 - 3035
反应条件
dichloro bis(acetonitrile) palladium(II); triethylamine in tetrahydrofuran multistep reaction: 1.) -78 deg C, 2.) -60 deg C -> room temperature; palladium-assisted alkylation of various olefin with carbanions accompanied by reductive or β-elimination isolation procedure; stereo- and regioselectivity; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4973
