54509-73-8合成路线 (共 3623 条)
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane T=50°C; metathesis; P=7500.6 Torr; 2 h;
参考文献
Warwel, Siegfried; Bruese, Falk; Demes, Christoph; Kunz, Michael; Klaas, Mark Ruesch gen
Chemosphere, 2001 , vol. 43, # 1 p. 39 - 48
反应条件
aluminium trichloride
参考文献
Kosower,E.M.; Wu,G.-S.
Journal of Organic Chemistry, 1963 , vol. 28, p. 633 - 638
反应条件
hydrogenchloride; silicon grains; copper(l) chloride T=259.84°C; 5 h;
参考文献
Okamoto, Masaki; Onodera, Satoshi; Yamamoto, Yuji; Suzuki, Eiichi; Ono, Yoshio
Journal of the Chemical Society, Dalton Transactions, 2001 , # 1 p. 71 - 78
反应条件
dihydrogen hexachloroplatinate; dichloromonosilane
参考文献
Union Carbide and Carbon Corp.
Patent: US2637738 , 1949 ;
反应条件
in neat (no solvent) H2SiCl2/HSiCl3 mixt. and C2H4 above 100°C in presence of Pt;;
参考文献
Gmelin Handbook: Si: MVol.C, 51, page 146 - 149
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Union Carbide & Carbon Corp.
Patent: US2637738 , 1953 ;
C. A., 1954 , p. 8254
反应条件
aluminium chloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane
参考文献
Dr. Karl Thomae GmbH
Patent: US4584293 A1, 1986 ;
反应条件
(i) AlCl3, CH2Cl2, (ii) /BRN= 1730731/; Multistep reaction;
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 22 p. 6160 - 6163
反应条件
aluminium trichloride in dichloromethane 4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Kanao, Munefumi; Hashizume, Takeshi; Ichikawa, Yoshifumi; Irie, Kiyoshi; Isoda, Sumiro
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1358 - 1363
反应条件
aluminium trichloride in dichloromethane Cyclization;
参考文献
Nevy, John B.; Hawkinson, David C.; Blotny, Grzegorz; Yao, Xudong; Pollack, Ralph M.
Journal of the American Chemical Society, 1997 , vol. 119, # 52 p. 12722 - 12726
反应条件
aluminium trichloride in dichloromethane 2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 22 p. 6160 - 6163