54509-73-8 合成路线 （共 3623 条）
反应条件
aluminium trichloride
参考文献
Baddeley et al.
参考文献
Catch et al.
反应条件
aluminium trichloride 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, RT, 18 h; Yield given. Multistep reaction;
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
反应条件
aluminium trichloride in dichloromethane 1.) -27 deg C, 30 min, 2.) -10 deg C, 1 h, 3.) 0-5 deg C, 1 h, H2O; further temperatures;
参考文献
Fivush, Adam M.; Strunk, Sanford R.
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) in ethanol T=110°C; P=37503 Torr; 1 h;
参考文献
Jones, M. D.
反应条件
1: ethene With n-butyllithium; zirconocene dichloride Metallation; 2: 1-bromohex-1-yne With copper(l) chloride T=20°C; Metallation; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 21 p. 6951 - 6957
→
反应条件
17741-60-5 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-二十一氟十二烷醇丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
反应条件
Yield given. Multistep reaction;
参考文献
Hegedus,L.S.; Darlington,W.H.
