54509-73-8 合成路线 (共 3623 条)
参考文献
Titow; Makljaew
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 1631,1634;engl.Ausg.S.1613
参考文献
Journal of Organic Chemistry, , vol. 22, p. 639,641
Angewandte Chemie, , vol. 69, p. 124,126
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反应条件
17741-60-5 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-二十一氟十二烷醇丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9 ;
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
反应条件
dichloro bis(acetonitrile) palladium(II); triethylamine 1.) THF, -78 deg C, 2.) -60 deg C -> room temperature; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4973
反应条件
aluminium trichloride
参考文献
DAINIPPON INK AND CHEMICALS, INC.
Patent: EP1201632 A1, 2002 ;
反应条件
AlCl3, aluminium chloride
参考文献
DAINIPPON INK AND CHEMICALS, INC.
Patent: EP1191008 A1, 2002 ;
Location in patent: Page 68 ;
反应条件
tetrabutylammomium bromide; iodine in dichloromethane T=20°C; 50 h;
参考文献
Rozhkov, I. N.; Igumnov, S. M.; Pletnev, S. I.; Chaplina, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 4.2 p. 856
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 4 p. 951
反应条件
T=140°C; P=11250.9 Torr; 2 h; various CC-unsaturated compounds investigated; Product distribution;
参考文献
Probst, A.; Raab, K.; Ulm, K.; Werner, K. von
Journal of Fluorine Chemistry, 1987 , vol. 37, p. 223 - 246