54509-73-8合成路线 （共 3623 条）
反应条件
T=15°C; 1 h; Irradiation; Product distributionKineticsMechanism;
参考文献
Tanko, James M.; Skell, Philip S.; Seshadri, Sri
Journal of the American Chemical Society, 1988 , vol. 110, # 10 p. 3221 - 3225
反应条件
Irradiation; Product distributionMechanismKinetics;
参考文献
Tanko, James M.; Skell, Philip S.; Seshadri, Sri
Journal of the American Chemical Society, 1988 , vol. 110, # 10 p. 3221 - 3225
反应条件
T=220°C; 20 h; other cyclic and acyclic dienophiles; Mechanism;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 1 p. 81 - 85
Khimiya Geterotsiklicheskikh Soedinenii, , # 1 p. 95 - 100
参考文献
Birckenbach; Linhard
Chemische Berichte, 1929 , vol. 62, p. 2263,2273
Full Text Show Details
Birckenbach; Linhard
Chemische Berichte, 1931 , vol. 64, p. 961,965
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
反应条件
in hydrogenchloride; ethanol; water byproducts: KCl; other Radiation; Pt complex dissolved in a mixt. of h2O, EtOH and concd.HCl (1:1:1), vessel pressurized with ethene (50 psi), sealed, heated in a microwave oven at 130°C for 15 min; cooled to 50°C, evapd., extd.(acetone) 2 times, cooled to 0°C, filtered, evapd.;
参考文献
Shoemaker, Krista A.; Leadbeater, Nicholas E.
Inorganic Chemistry Communications, 2009 , vol. 12, # 5 p. 341 - 342
反应条件
n-butyl-magnesium chloride; zirconocene dichloride in tetrahydrofuran T=80°C; P=760 Torr; 0.666667 h;
参考文献
Terao, Jun; Torii, Kazushi; Saito, Koyu; Kambe, Nobuaki; Baba, Akio; Sonoda, Noboru
Angewandte Chemie - International Edition, 1998 , vol. 37, # 19 p. 2653 - 2656
反应条件
triethylamine; PdCl2{P(OC6H5)3}2 in carbon dioxide Mizoroki-Heck reaction; P=19000 Torr; Product distribution; Further Variations:Pressures;
参考文献
Kayaki; Noguchi; Ikariya
Chemical Communications, 2000 , # 22 p. 2245 - 2246
反应条件
CO in hexane under N2; Ru compd. is dissolved in hexane, transferred to a Hoke cylinder, charged with CO (1 atm) and ethylene (3 atm), allowed to sit at room temp. for 20 h; gases are vented, IR, mixt. is reduced in volume, cooled to -20°C: crystn. of Ru3(CO)12, soln. is filtered after 12 h, reduced in volume to half, IR, soln. is cooled to -20°C, supernatant liq. is similar worked up; elem. anal.;
参考文献
Journal of Molecular Catalysis, , vol. 21, p. 297 - 312
反应条件
CO in hexane under N2; Ru compd. is dissolved in hexane, transferred to a Hoke cylinder, charged with CO (1 atm) and ethylene (3 atm), allowed to sit at room temp. for 20 h; gases are vented, IR, mixt. is reduced in volume, cooled to -20°C: crystn. of Ru3(CO)12, soln. is filtered after 12 h, reduced in volume to half, IR, soln. is cooled to -20°C, supernatant liq. is similar worked up; elem. anal.;
参考文献
Kampe, C. E.; Boag, N. M.; Kaesz, H. D.
Journal of Molecular Catalysis, 1983 , vol. 21, p. 297 - 312
