54509-73-8合成路线 （共 3623 条）
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide
T=105°C; Heck-Mizoroki reaction; P=775.743 Torr; 16 h; Inert atmosphere;
参考文献
Smith, Craig R.; RajanBabu
Tetrahedron, 2010 , vol. 66, # 5 p. 1102 - 1110
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl acetamide
T=60°C; P=775.743 Torr; 12 h;
参考文献
Saini, Vaneet; Liao, Longyan; Wang, Qiaofeng; Jana, Ranjan; Sigman, Matthew S.
Organic Letters, 2013 , vol. 15, # 19 p. 5008 - 5011
反应条件
1,2,3,4-tetrahydro-naphthalene
T=270 - 280°C;
参考文献
Rocek,J.; Aylward,D.E.
Journal of the American Chemical Society, 1975 , vol. 97, p. 5452 - 5456
反应条件
potassium carbonate in toluene
T=140°C;
参考文献
Bestian,H.; Guenther,D.
Angewandte Chemie, 1963 , vol. 75, p. 841 - 845
反应条件
silicon; copper(l) chloride in di-isopropyl ether
T=513°C; phenol 26 kPa, ethylene 81 kPa; Yield given;
参考文献
Okamoto, Masaki; Watanabe, Naoto; Suzuki, Eiichi; Ono, Yoshio
Journal of Organometallic Chemistry, 1996 , vol. 515, # 1-2 p. 51 - 55
反应条件
(i) BH3, THF, (ii) /BRN= 2078967/, MeI, K2CO3; Multistep reaction;
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 4166 - 4168
反应条件
1: toluene With n-butyllithium; LiK(OCH2CH2NMe2)2; Mg(OCH2CH2OEt)2 in various solvent(s)
T=20°C; Metallation; 0.5 h;
2: ethene in various solvent(s)
T=80°C; Alkylation; P=7600.51 Torr; 24 h; Further stages.;
参考文献
Steele, Barry R.; Screttas, Constantinos G.
Journal of the American Chemical Society, 2000 , vol. 122, # 10 p. 2391 - 2392
反应条件
phenanthrene; sodium; lithium in tetrahydrofuran
T=22°C; P=760.051 Torr; 24 h; Inert atmosphere;
参考文献
Rummel; Yunusov; Kalyuzhnaya; Shur
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1467 - 1472
反应条件
naphthalene; sodium; lithium in tetrahydrofuran
T=22°C; P=760.051 Torr; 24 h; Inert atmosphere;
参考文献
Rummel; Yunusov; Kalyuzhnaya; Shur
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1467 - 1472
反应条件
phenanthrene; sodium; lithium in tetrahydrofuran
T=22°C; P=760.051 Torr; 24 h; Inert atmosphere;
参考文献
Rummel; Yunusov; Kalyuzhnaya; Shur
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1467 - 1472
