54509-73-8合成路线 （共 3623 条）
反应条件
manganese in N,N-dimethyl-formamide T=60°C;
参考文献
Journal of Fluorine Chemistry, , vol. 28, p. 229 - 234
参考文献
AlliedSignal Inc.
Patent: US6300532 B1, 2001 ;
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; potassium tert-butylate 1.) hexane, -25 deg C, 2 h, 2.) THF, -30 deg C; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 3 p. 260 - 261
反应条件
pentacarbonyliron(0); water T=120 - 140°C; P=125036 - 147102 Torr;
参考文献
BASF
Patent: DE839800 , 1943 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
反应条件
pentacarbonyliron(0); water T=120 - 140°C; P=125036 - 147102 Torr;
参考文献
BASF
Patent: DE839800 , 1943 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
反应条件
T=120 - 140°C; P=125036 - 132391 Torr;
参考文献
Reppe
Experientia, 1949 , vol. 5, p. 109
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 7-9,17
Full Text Show Details
Reppe,W.
Acetylene Chemistry <New York 1949>S.179,180
Full Text Show Details
Basf
Patent: DE839800 , 1943 ;
Full Text Show Details
Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
反应条件
T=120 - 125°C; P=139746 - 147102 Torr;
参考文献
BASF
Patent: DE839800 , 1943 ;
Full Text Show Details
Reppe; Vetter
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 135,148
Full Text Show Details
BASF
Chem. Zentralbl., 1952 , vol. 123, p. 6762
参考文献
Weeks, P.; Gard, G. L.
Journal of Fluorine Chemistry, 1971 , vol. 1, p. 295 - 307
反应条件
dibenzoyl peroxide T=80°C; 18 h;
参考文献
Seyferth; Simon; Sepelak; Klein
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4634 - 4639
反应条件
dibenzoyl peroxide T=65 - 110°C; P=5171.62 - 10343.2 Torr; 24 h;
参考文献
Honeywell International Inc.
Patent: US2007/161827 A1, 2007 ;
Location in patent: Page/Page column 3 ;
