54509-73-8合成路线 （共 3623 条）
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=100°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Albahily, Khalid; Gambarotta, Sandro; Duchateau, Robbert
Organometallics, 2011 , vol. 30, # 17 p. 4655 - 4664
反应条件
RuCl2(PCy3)2(3-phenyl-1H-inden-1-ylidene) in dichloromethane Grubbs Olefin Metathesis; P=6000.6 Torr; 6 h; Schlenk techniqueInert atmosphere;
参考文献
Julis, Jennifer; Bartlett, Stuart A.; Baader, Sabrina; Beresford, Nicola; Routledge, Edwin J.; Cazin, Catherine S.J.; Cole-Hamilton, David J.
Green Chemistry, 2014 , vol. 16, # 5 p. 2846 - 2856
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; potassium tert-butylate 1.) hexane, -25 deg C, 2 h, 2.) THF, -30 deg C; Yield given. Multistep reaction;
参考文献
Brandsma, Lambert; Verkruijsse, Hermann D.; Schade, Christian; Rague Schleyer, Paul von
Journal of the Chemical Society, Chemical Communications, 1986 , # 3 p. 260 - 261
反应条件
aluminum oxide; tetramethylstannane; Re2O7 in chlorobenzene T=19.9°C; P=1500.1 Torr; 20 h; var. of catalyst, ratio substrate : catalyst, solvent, temp., pressure; Product distribution;
参考文献
Bosma, Ruud H. A.; Aardweg, Fred van den; Mol, Johannes C.
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1132 - 1133
反应条件
Cl2(PCy3)(N,N'-(Mes)2-imidazolidin-2-yl)Ru=CHC6H5 T=20°C; 12 h; Product distribution / selectivity;
参考文献
EP1251135 A2, ;
Page 16-17 ;
参考文献
Colubchenko, I. T.; Galoch, P. N.; Gutyrya, V. S.; Motornyi, V. G.; Khranovskaya, V. I.
Doklady Chemistry, 1981 , vol. 261, p. 521 - 523
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 261, # 4 p. 891 - 894
反应条件
tetramethylstannane; [MoCl5]; silica gel T=27°C; Kinetics; Further Variations:Temperatures;
参考文献
Bykov; Belyaev; Butenko; Finkel'shtein
Petroleum Chemistry, 2005 , vol. 45, # 6 p. 429 - 432
反应条件
acetone in benzene-d6 2 mol equiv. acetone and 2 mol equiv. C2H4 condensed into NMR tube contg. 1 mol equiv. soln. W-complex/C6D6 at -196°C, tube sealed; not isolated, detected by NMR-spect.; other uncharacterized products also present;
参考文献
Organometallics, , vol. 11, p. 3965 - 3970
参考文献
Shostenko,A.G. et al.
Zhurnal Organicheskoi Khimii, 1979 , vol. 15, # 3 p. 458 - 463,405 - 410
反应条件
1,2-diphenyl-1-keto-2,2-dimethoxyethane T=45°C; P=2250.23 - 6750.68 Torr; 14.1 h; UV-irradiation;
参考文献
Hebert, Melanie; Ollivier, Jean; Fremy, Georges
Patent: US2005/40028 A1, 2005 ;
Location in patent: Page/Page column 2 ;
