54509-73-8合成路线 (共 3623 条)
反应条件
aluminium trichloride in dichloromethane
参考文献
Lamberts, Joseph J. M.; Cuppen, Theo J. H. M.; Laarhoven, Wim H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1819 - 1828
反应条件
aluminium trichloride in dichloromethane T=-78°C; 8 h; Irradiation; Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 30, # 45 p. 6193 - 6194
反应条件
aluminum tri-bromide in dichloromethane T=-78°C; 7.5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Kakiuchi, Kiyomi; Yamaguchi, Bunji; Kinugawa, Masahiko; Ue, Masaki; Tobe, Yoshito; Odaira, Yoshinobu
Journal of Organic Chemistry, 1993 , vol. 58, # 10 p. 2797 - 2803
反应条件
aluminium trichloride in dichloromethane T=-78°C; 8 h; Irradiationvarious catalyst type Lewis acid; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 45 p. 6193 - 6194
反应条件
in neat (no solvent) byproducts: HCl, H2; Irradiation (UV/VIS); irradiating SiH2Cl2-C2H4 gas mixt. with CO2 laser at atmospheric pressure (reaction flame temp. from less than 1273 K to more than 3073 K depending on power density and C2H4/SiH2Cl2 ratio); X-ray powder diffraction, transmission electron microscopy;
参考文献
Suzuki, M.; Nakata, Y.; Okutani, T.; Kato, A.
Journal of Materials Science, 1992 , vol. 27, p. 6091 - 6097
反应条件
in neat (no solvent) byproducts: H2; decompn. at 332 °C;;
参考文献
Emeleus, H. J.; Reid, C.
Journal of the Chemical Society, 1939 , p. 1021 - 1030
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Gmelin Handbook: Si: MVol.B, 65, page 253 - 255
反应条件
anschl. mit Kohlendioxid;
参考文献
Job; Reich
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1923 , vol. 177, p. 1439
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Job; Reich
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1924 , vol. 179, p. 331
反应条件
[CrCl2(THF)2]; Ph2PN(Me)(CH2)3N(Me)PPh2 in 2-methyl cyclohexane T=80°C; P=30003 Torr; 0.5 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 6 p. 1366 - 1369
反应条件
methylaluminoxane; C64H58Cl6Cr2N2O2P4 in N-dodecane; toluene T=25°C; P=3040.2 Torr; 1.5 h; Product distribution / selectivity;
参考文献
WO2009/46144 A1, ;
Page/Page column 16-19 ;
反应条件
Cr(DMPMNBz)Cl3 in toluene T=80°C; P=15201 Torr; 0.25 h; Gas phaseAutoclave; Product distribution / selectivity;
参考文献
US2012/178939 A1, ;
Page/Page column 5-6 ;