54509-73-8合成路线 (共 3623 条)
反应条件
methanesulfonic acid; palladium diacetate; bis(phosphaadamantyl)diphosphine T=90°C;
参考文献
Pugh; Drent; Pringle
Chemical Communications, 2001 , # 16 p. 1476 - 1477
反应条件
ruthenium trichloride; tetraethylammonium iodide in N,N-dimethyl-formamide T=190°C; P=45003.6 Torr; 1 h; var. solvents, reaction times, promoters, and ruthenium complexes, also in the presence of CO; Product distribution;
参考文献
Urry; Huyser
Journal of the American Chemical Society, 1953 , vol. 75, p. 4876
反应条件
pyridine; carbon monoxide; palladium diacetate in methanol
参考文献
Shell Oil Company
Patent: US5166411 A1, 1992 ;
反应条件
lithium iodide; hexacarbonyl molybdenum in tetrahydrofuran; methanol
参考文献
The Halcon SD Group, Inc.
Patent: US4540811 A1, 1985 ;
反应条件
T=-80.16 - 49.84°C; P=3000.3 Torr; 0.0133333 h;
参考文献
Journal of Organometallic Chemistry, , vol. 745-746, p. 115 - 119
反应条件
methanol; 1-(di-tert-butylphosphinomethyl)-2-(di-o-tolylphosphinomethyl)benzene; palladium diacetate T=100°C; P=15001.5 Torr; 3 h; Product distribution / selectivity;
参考文献
LUCITE INTERNATIONAL UK LIMITED; EASTHAM, Graham Ronald; WAUGH, Mark; PRINGLE, Paul; FANJUL SOLARES, Tamara
Patent: WO2010/1174 A1, 2010 ;
Location in patent: Page/Page column 65; 66 ;
反应条件
cobalt T=250°C; P=478080 - 551631 Torr;
参考文献
Du Pont de Nemours and Co.
Patent: US2542767 , 1949 ;
反应条件
methanesulfonic acid; hydrogen; Pd(OAc)2*1,2-bis(di-s-butylphosphino)ethane T=120°C;
参考文献
Pugh, Robert I.; Drent, Eite
Advanced Synthesis and Catalysis, 2002 , vol. 344, # 8 p. 837 - 840
反应条件
Ph3P(+)CH3I(-); triphenylphosphine; Rhodium trichloride in various solvent(s) T=180°C; P=60004.8 Torr; 4 h; further ereaction conditions and promotors; Product distribution;
参考文献
Tetrahedron Letters, , vol. 32, # 32 p. 3989 - 3992
反应条件
methanesulfonic acid; Pd(DBPMB)(DBA) T=80°C; P=7500.75 Torr; 2 h;
参考文献
Eastham, Graham R.; Tooze, Robert P.; Kilner, Melvyn; Foster, Douglas F.; Cole-Hamilton, David J.
Journal of the Chemical Society, Dalton Transactions, 2002 , # 8 p. 1613 - 1617