54509-73-8合成路线 （共 3623 条）
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; sodium hydrogencarbonate in tert-butyl alcohol T=80°C; P=413.729 Torr; 4 h;
参考文献
Saini, Vaneet; Liao, Longyan; Wang, Qiaofeng; Jana, Ranjan; Sigman, Matthew S.
Organic Letters, 2013 , vol. 15, # 19 p. 5008 - 5011
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; phosphate potassium salt in 1,1-dimethylpropan-1-ol T=80°C; P=413.729 Torr; 12 h;
参考文献
Saini, Vaneet; Liao, Longyan; Wang, Qiaofeng; Jana, Ranjan; Sigman, Matthew S.
Organic Letters, 2013 , vol. 15, # 19 p. 5008 - 5011
反应条件
1: ethene; para-iodoanisole With palladium diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; 2-dicyclohexylphosphino-1,1'-biphenyl in N,N-dimethyl-formamide; toluene T=120°C; Mizoroki-Heck coupling; P=11251.1 Torr; 0.333333 h; 2: 4-trifluoromethyl-1-iodobenzene With palladium diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; 2-dicyclohexylphosphino-1,1'-biphenyl in N,N-dimethyl-formamide; toluene T=120°C; Heck reaction; P=15001.5 Torr;
参考文献
Bourne, Samuel L.; Koos, Peter; Obrien, Matthew; Martin, Benjamin; Schenkel, Berthold; Baxendale, Ian R.; Ley, Steven V.
Synlett, 2011 , # 18 p. 2643 - 2647
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in toluene T=110°C; 2 h;
参考文献
Ferre-Filmon, Karine; Delaude, Lionel; Demonceau, Albert; Noels, Alfred F.
European Journal of Organic Chemistry, 2005 , # 15 p. 3319 - 3325
反应条件
sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=90°C; Heck reaction; P=7600.51 Torr; 0.5 h; Inert atmosphereAutoclave;
参考文献
Applied Organometallic Chemistry, , vol. 25, # 4 p. 289 - 293
反应条件
tert.-butylnitrite; palladium diacetate in dichloromethane; acetic acid 18 h; Ambient temperature;
参考文献
Beller, Matthias; Fischer, Hartmut; Kuehlein, Klaus
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8773 - 8776
反应条件
sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide Heck reaction; P=3800.26 Torr; Inert atmosphereAutoclave;
参考文献
Applied Organometallic Chemistry, , vol. 25, # 4 p. 289 - 293
反应条件
in octane refluxed 3 h passing C2H4 through soln.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 407 - 412
反应条件
in hexane Os-cluster and ligand were placed in tube with hexane, heated for 15 h at 100°C 1.5 bar under N2; solvent and volatiles were removed in vacuo, TLC with hexane-CH2Cl2;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 6 p. 1020 - 1023
反应条件
aluminum oxide; ammonia; CaO T=400 - 1000°C;
参考文献
I.G.Farbenind.
Patent: US1919761 , 1931 ;
Full Text Show Details
I.G.Farbenind.
Patent: FR717567 ;
