54509-73-8合成路线 (共 3623 条)
反应条件
Irradiation (UV/VIS); λ=253.7 nm; products found by gas chromy.;
参考文献
Dzantiev, B. G.; Shiskov, A. V.; Unukovich, M. S.
High Energy Chem. (USSR), 1968 , vol. 2, p. 492 - 493
Khim. Vysokikh Energ., 1968 , vol. 2, p. 570 - 572
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.3.1.1, page 146 - 150
反应条件
[Co4(CO)11{P(OPh)3}] T=85°C; Cycloaddition; Pauson-Khand reaction; P=152000 - 159600 Torr; 42 h;
参考文献
Jeong, Nakcheol; Hwang, Sung Hee
Angewandte Chemie - International Edition, 2000 , vol. 39, # 3 p. 636 - 638
反应条件
tris(n-butyl)phosphine oxide in toluene T=110°C; P=38000 Torr; 36 h;
参考文献
Billington, David C.; Helps, I. Malcolm; Pauson, Peter L.; Thomson, William; Willison, Debra
Journal of Organometallic Chemistry, 1988 , vol. 354, p. 233 - 242
反应条件
dicobalt octacarbonyl in toluene T=150°C; P=232519 - 270022 Torr; 16 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Rautenstrauch, Valentin; Megard, Patrick; Conesa, Jose; Kuester, Wilhelm
Angewandte Chemie, 1990 , vol. 102, # 12 p. 1441 - 1443
反应条件
trimethylamine-N-oxide 1.) petroleum ether, RT, 4 h, 2.) toluene, MeOH, from 25 to 30 atm, 40 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Donkervoort, Johannes G.; Gordon, Alison R.; Johnstone, Craig; Kerr, William J.; Lange, Udo
Tetrahedron, 1996 , vol. 52, # 21 p. 7391 - 7420
反应条件
dicobalt octacarbonyl in toluene T=150°C; P=232519 - 270022 Torr; 16 h; variation of cond.; Mechanism;
参考文献
Rautenstrauch, Valentin; Megard, Patrick; Conesa, Jose; Kuester, Wilhelm
Angewandte Chemie, 1990 , vol. 102, # 12 p. 1441 - 1443
参考文献
Albisetti et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 1489,1492
反应条件
isoquinoline; lithium chloride; palladium dichloride in various solvent(s) T=160°C;
参考文献
Goossen, Lukas J.; Paetzold
Angewandte Chemie - International Edition, 2002 , vol. 41, # 7 p. 1237 - 1241
反应条件
(10H)-phenothiazine; bis(.mu.-chloro)bis{(2-(1-(hydroxyimino)methyl)phenyl-C1,N)palladium(II)}; potassium acetate in N,N-dimethyl acetamide T=105°C; Heck-Mizoroki reaction; P=775.743 Torr; 10 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 66, # 5 p. 1102 - 1110
反应条件
T=270°C; P=3750.38 Torr; Conversion of starting material;
参考文献
Institut Francais du Petrole
Patent: US7081558 B2, 2006 ;
Location in patent: Page/Page column 9 ;