54509-73-8合成路线 (共 3623 条)
反应条件
methylalumoxane (PMAO-S) in toluene T=45°C; P=15001.5 Torr; 1 h; Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2006/293546 A1, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
hydrogen; [4-methyl-N1-phenyl-N2-(diphenylphosphino)benzamidine](THF)CrCl3 in n-heptane; ethylbenzene T=50°C; P=43958.7 Torr; 0.5 h; Product distribution / selectivity;
参考文献
CHEVRON PHILLIPS CHEMICAL COMPANY LP; SYDORA, Orson L; CARNEY, Michael; SMALL, Brooke L; HUTSHISON, Steven; GEE, Jeffery C
Patent: WO2011/82192 A1, 2011 ;
Location in patent: Page/Page column 356-359; 369 ;
反应条件
trichloro(.eta.5-cyclopentadienyl)titanate(1-); methylaluminoxane; trimethylaluminum in toluene T=35°C; P=7500.75 Torr; 1 h; Product distribution / selectivity;
参考文献
TOTAL PETROCHEMICALS RESEARCH FELUY
Patent: EP1832597 A1, 2007 ;
Location in patent: Page/Page column 11-13 ;
反应条件
triphenylphosphine; bis(1,5-cyclooctadiene)nickel (0) in toluene T=25°C; P=22502.3 Torr; 24 h; Product distribution; Further Variations:TemperaturesCatalystsPressures;
参考文献
Dalton Transactions, , # 6 p. 822 - 831
反应条件
Cr((Me2pz)2CHSiMe2N(H)(i)Pr)Cl2(THF) in toluene T=60°C; P=26252.6 Torr; Autoclave;
参考文献
Albahily, Khalid; Gambarotta, Sandro; Duchateau, Robbert
Organometallics, 2011 , vol. 30, # 17 p. 4655 - 4664
反应条件
methylalumoxane (PMAO-S) in toluene T=80°C; P=15001.5 Torr; 1 h; Product distribution / selectivity;
参考文献
Braunstein, Pierre; Chauvin, Yves; Mercier, Sophie; Saussine, Lucien; Cian, Andre De; Fischer, Jean
Journal of the Chemical Society, Chemical Communications, 1994 , # 19 p. 2203 - 2204
反应条件
1: With tri(n-octyl)aluminium in toluene T=80°C; 2: With CrCl3(THF)3; bis(di{ortho-methoxyphenyl}phosphanyl)(methyl)amine in toluene T=80°C; 1 h; Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2006/293546 A1, 2006 ;
Location in patent: Page/Page column 7-8 ;
反应条件
1: in toluene T=40°C; P=3750.38 Torr; 0.5 h; AutoclaveInert atmosphere; 2: With ethanol Product distribution / selectivity;
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED; SENDA, Taichi; TANIMOTO, Masaya; HANAOKA, Hidenori
Patent: WO2012/133924 A1, 2012 ;
Location in patent: Page/Page column 52 ;
反应条件
1: With [(t-Bu)NP(Ph)2N(t-Bu)]Cr(μ2-Cl)2Li(THF)2 in toluene T=60°C; P=26252.6 Torr; 1 h; Inert atmosphere; 2: With hydrogenchloride in ethanol; toluene
参考文献
Shaikh, Yacoob; Gurnham, Joanna; Albahily, Khalid; Gambarotta, Sandro; Korobkov, Ilia
Organometallics, 2012 , vol. 31, # 21 p. 7427 - 7433,7
反应条件
in toluene P=52505.3 Torr; Inert atmosphereSchlenk techniqueAutoclave;
参考文献
Journal of Organometallic Chemistry, , vol. 720, p. 73 - 80,8
Journal of Organometallic Chemistry, , vol. 720, p. 73 - 80