54509-73-8合成路线 (共 3623 条)
反应条件
lt;Zr(η-butadiene)2(dmpe)gt;2(dmpe) (dmpe = 1,2-bis(dimethylphosphino)ethane) in toluene T=70°C; 50 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 3 p. 353 - 366
反应条件
pentane T=200 - 220°C; P=294203 - 330978 Torr;
参考文献
Ziegler; Gellert
Patent: DE878560 , 1950 ;
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Ziegler; Gellert
Patent: US2699457 , 1951 ;
反应条件
tetramethyldialuminoxane; [Ni{1-N(PMes2)-2-N-(μ-PMes2)C6H4-κ3N,N',P,-κ1P'}]2 in toluene T=25°C; P=15201 Torr; 3 h; Product distribution; Further Variations:SolventsNi/Al ratio;
参考文献
Majoumo-Mbe, Felicite; Loennecke, Peter; Volkis, Victoria; Sharma, Manab; Eisen, Moris S.; Hey-Hawkins, Evamarie
Journal of Organometallic Chemistry, 2008 , vol. 693, # 15 p. 2603 - 2609
反应条件
in tetrahydrofuran T=23°C; P=775.743 Torr; 24 h; GloveboxSchlenk technique; TemperatureTimePressure;
参考文献
Dalton Transactions, , vol. 42, # 25 p. 9198 - 9210
反应条件
methylaluminoxane; [2-Ph2PCH2-4,4-Me2-4,5-dihydrooxazole]CoCl2 in toluene T=25°C; P=7500.75 Torr; 0.583333 h; Product distribution; Further Variations:CatalystsReagents;
参考文献
Dalton Transactions, , # 39 p. 4472 - 4482
反应条件
ethylaluminum dichloride; [Ni(μ-Cl){(4,5-dihydro-4,4-Me2-oxazol-2-yl)methanol}]2Cl2 in chlorobenzene T=25 - 30°C; P=7500.75 Torr; 0.583333 h; Product distribution; Further Variations:Catalystscatalyst-co-catalyst ratio; catalyt amount;
参考文献
Dalton Transactions, , # 12 p. 1564 - 1573
反应条件
(i-PrC5H4)2Ni; ethylaluminum dichloride in toluene T=69.9°C; P=2250.2 Torr; other nickel catalysts; Product distribution;
参考文献
Sauthier, Mathieu; Leca, Francois; De Souza, Roberto Fernando; Bernardo-Gusmao, Katia; Trevisan Queiroz, Luiz Fernando; Toupet, Loic; Reau, Regis
New Journal of Chemistry, 2002 , vol. 26, # 5 p. 630 - 635
反应条件
C58H54N3NiO3P in toluene T=30°C; P=4125.41 Torr; 0.5 h; Kinetics; TemperatureReagent/catalyst;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 9-10 p. 1254 - 1258
反应条件
Pd(II)-cyclic α-diphenylphosphino-ketoimine in dichloromethane T=70°C; P=7500.6 Torr; 2 h; Product distribution; Further Variations:CatalystsPressuresSolvents;
参考文献
Keim, Wilhelm; Killat, Stefan; Nobile, Cosimo F; Suranna, Gian Paolo; Englert, Ulli; Wang, Ruimin; Mecking, Stefan; Schroeder, Dirk Lucas
Journal of Organometallic Chemistry, 2002 , vol. 662, # 1-2 p. 150 - 171
反应条件
methylaluminoxane; 2,9-diCHO-1,10-phenanthrolinebis(2,4,6-triMeanil)CoCl2 in toluene T=120.27°C; P=15001.2 Torr; Product distribution; Further Variations:ReagentsTemperaturesPressures;
参考文献
Journal of Organometallic Chemistry, , vol. 658, # 1-2 p. 62 - 70