54509-73-8合成路线 （共 3623 条）
反应条件
di-tert-butyl peroxide T=140 - 150°C; Product distribution;
参考文献
Germash, A. V.; Dostovalova, V. I.; Zorin, V. V.; Terent'ev, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 1 p. 149 - 153
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 1 p. 173 - 178
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=120°C; P=22800 Torr; 24 h;
参考文献
Kasahara, Akira; Izumi, Taeko; Murakami, Satoshi; Miyamoto, Kazuhiro; Hino, Toshimi
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1405 - 1413
反应条件
palladium diacetate; triethylamine 1.) toluene, reflux 2.) toluene, reflux, 35 min; Yield given. Multistep reaction;
参考文献
Horino, Hiroshi; Inoue, Naoto
Journal of Organic Chemistry, 1981 , vol. 46, p. 4416 - 4422
反应条件
di-tert-butyl peroxide
参考文献
Finke,M.; Kleiner,H.-J.
Justus Liebigs Annalen der Chemie, 1974 , p. 741 - 750
反应条件
K2Ru4/H2 T=20°C; P=600 Torr; 0.3 h; Sealed tube; Reagent/catalystTime;
参考文献
Yunusov; Rummel; Herrmann; Kalyuzhnaya; Shur
Russian Chemical Bulletin, 2013 , vol. 62, # 5 p. 1191 - 1194
Izv. Akad. Nauk, Ser. Khim., 2013 , vol. 62, # 5 p. 1191 - 1194,4
反应条件
(i), (ii) aq. NaOH; Multistep reaction;
参考文献
Whitney; Gregory; Kauer; Roland; Snyder; Benson; Hermann
Journal of medicinal chemistry, 1970 , vol. 13, # 2 p. 254 - 260
反应条件
tris-(dibenzylideneacetone)dipalladium(0); hypophosphorous ether; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene T=80 - 100°C; Reagent/catalystSolvent;
参考文献
Clariant Finance (BVI) Limited; Hill, Michael; Bauer, Harald; Krause, Werner; Sicken, Martin
Patent: US8664418 B2, 2014 ;
Location in patent: Page/Page column 25 ;
反应条件
in tetrahydrofuran C2H4-atmosphere, 12 h; evapn. (vac.);
参考文献
Bennett, Martin A.; Johnson, Julian A.; Willis, Anthony C.
Organometallics, 1996 , vol. 15, # 1 p. 68 - 74
反应条件
(i) Cl2, (ii) H2O; Multistep reaction;
参考文献
Beger,J. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 15 - 35
参考文献
Tarasova,N.P. et al.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 1 p. 19 - 22,15 - 17
