吡啶-2.6-二羧酸二甲酯合成路线 (共 63 条)
反应条件
hydrogenchloride in methanol 4 h; Reflux;
参考文献
Journal of Coordination Chemistry, , vol. 63, # 14-16 p. 2400 - 2418
反应条件
1: 1.) n-butyllithium / 1.) THF, -89 deg C, 4 h, 2.) THF, from -89 deg C to RT 2: HCl / 24 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 186, # 2 p. 147 - 153
反应条件
1: Heating 2: 1.) Et4NBF4 / 1.) electrolysis, acetonitrile, 2.) acetonitrile, 24 h 3: Et4NBF4 / 1.) electrolysis, acetonitrile, 2.) acetonitrile, 24 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1365 - 1374
反应条件
1: 1.) Et4NBF4 / 1.) electrolysis, acetonitrile, 2.) acetonitrile, 24 h 2: Et4NBF4 / 1.) electrolysis, acetonitrile, 2.) acetonitrile, 24 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1365 - 1374
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 72, # 1 p. 198 - 203
参考文献
Journal of Molecular Structure, , vol. 1030, p. 19 - 25
反应条件
hydrogenchloride; n-butyllithium Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 186, # 2 p. 147 - 153
反应条件
tetraethylammonium tetrafluoroborate 1.) electrolysis, acetonitrile, 2.) acetonitrile, 24 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1365 - 1374
参考文献
Tetrahedron Letters, , vol. 54, # 43 p. 5771 - 5774
参考文献
Monatshefte fuer Chemie, , vol. 24, p. 199,200