吡啶-2.6-二羧酸二甲酯合成路线 （共 63 条）
反应条件
1: sodium tetrahydroborate / methanol / Cooling with ice 2: phosphorus tribromide / chloroform / 0 °C / Inert atmosphere View Scheme
参考文献
Goswami, Shymaprosad; Aich, Krishnendu; Das, Sangita; Das, Avijit Kumar; Sarkar, Deblina; Panja, Sukanya; Mondal, Tapan Kumar; Mukhopadhyay, Subhrakanti
Chemical Communications, 2013 , vol. 49, # 91 p. 10739 - 10741
反应条件
sodium tetrahydroborate in methanol
参考文献
Lewandowski, Bartosz; Jarosz, Slawomir
Organic Letters, 2010 , vol. 12, # 11 p. 2532 - 2535
反应条件
sodium tetrahydroborate in methanol Cooling with ice;
参考文献
Price, Eric W.; Cawthray, Jacqueline F.; Bailey, Gwendolyn A.; Ferreira, Cara L.; Boros, Eszter; Adam, Michael J.; Orvig, Chris
Journal of the American Chemical Society, 2012 , vol. 134, # 20 p. 8670 - 8683
反应条件
1.1: 48 percent / sodium borohydride / methanol / 5 h / Heating 2.1: EtONa / toluene / 5 h / Heating 2.2: 46 percent / aq. H2SO4 / 2 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 19 p. 3393 - 3402
反应条件
1.1: lithium borohydride / tetrahydrofuran / 16 h / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 2.2: 12 h View Scheme
参考文献
Dungan, Victoria J.; Poon, Belinda M.-L.; Barrett, Elizabeth S.; Rutledge, Peter J.
Tetrahedron Letters, 2013 , vol. 54, # 10 p. 1236 - 1238
反应条件
1: lithium borohydride / tetrahydrofuran / 16 h / Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine / pyridine / 16 h / Inert atmosphere View Scheme
参考文献
Gifu University
Patent: EP2511260 A1, 2012 ;
反应条件
1: 51 percent / DIBAL-H / CH2Cl2 / 3 h / -78 °C
2: 98 percent / pyridinium toluene-p-sulphonate / methanol
View Scheme
参考文献
Masiero, Stefano; Fini, Federico; Gottarelli, Giovanni; Spada, Gian Piero
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2736 - 2753
反应条件
1: benzene
2: aqueous hydriodic acid; red phosphorus
View Scheme
参考文献
Lukes; Pergal
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 36,43
反应条件
4 A molecular sieve; sodium methylate in methanol
Product distribution;
参考文献
Bradshaw, Jerald S.; Jones, Brian A.; Nielsen, Ralph B.; Spencer, Neil O.; Thompson, Patricia K.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 957 - 962
反应条件
perchloric acid; Fe(ClO4)2·6H2O; dihydrogen peroxide in water
T=0 - 20°C; Fenton Reaction; 3 h; regioselective reaction;
参考文献
Kupai, Jozsef; Huszthy, Peter; Katz, Marianna; Toth, Tuende
Arkivoc, 2012 , vol. 2012, # 5 p. 134 - 145
