2-溴-N,N-二甲基丙酰胺合成路线 （共 4 条）
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2006/113552 A2, 2006 ;
Location in patent: Page/Page column 37-38; 61 ;
反应条件
in diethyl ether
0.5 h; Yield given;
参考文献
Foulds, Christopher D.; Jaxa-Chamiec, Albert A.; O'Sullivan, Anthony C.; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 1 p. 21 - 28
反应条件
1: allyl-magnesium chloride With gallium(III) chloride in tetrahydrofuran; hexane
T=25°C; 0.333333 h;
2: 2-bromo-N,N-dimethylpropionamide With air; triethyl borane in tetrahydrofuran; hexane; water
2 h;
参考文献
Takami, Kazuaki; Usugi, Shin-Ichi; Yorimitsu, Hideki; Oshima, Koichiro
Synthesis, 2005 , # 5 art. no. E12304SS, p. 824 - 839
反应条件
triethyl borane; oxygen in tetrahydrofuran; water
2 h;
参考文献
Usugi, Shin-ichi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron Letters, 2001 , vol. 42, # 27 p. 4535 - 4538
