N,N-二乙基-1-萘羧酰胺合成路线 （共 22 条）
反应条件
1: 1.) TMEDA, triphenylmethyl chloride, sec-BuLi / 1.) ether, cyclohexane, -78 deg C, 1 h, 2.) a) -78 deg C, 1 h, b) room temp., 3 h
2: 93 percent / Zn, pyridine, 10percent KOH / Heating; overnight
View Scheme
参考文献
Harvey, Ronald G.; Cortez, Cecilia; Jacobs, Stephen A.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2120 - 2125
反应条件
1: s-BuLi; TMEDA / tetrahydrofuran
2: LDA / tetrahydrofuran / -78 - 20 °C
View Scheme
参考文献
Pradhan, Tarun Kanti; De, Asish; Mortier, Jacques
Tetrahedron, 2005 , vol. 61, # 38 p. 9007 - 9017
