1-[4-(2-羟基丙-2-基)苯基]乙酮合成路线 (共 17 条)
反应条件
1: 72 h
2: diethyl ether / 0.5 h / 0 °C
3: toluene / 1 h / 100 °C
4: cyclohexane / 1 h / 250 °C
View Scheme
参考文献
Thomas, Alan F.; Perret, Celia
Tetrahedron, 1986 , vol. 42, # 12 p. 3311 - 3322
反应条件
1: diethyl ether / 0.5 h / 0 °C
2: toluene / 1 h / 100 °C
3: cyclohexane / 1 h / 250 °C
View Scheme
参考文献
Thomas, Alan F.; Perret, Celia
Tetrahedron, 1986 , vol. 42, # 12 p. 3311 - 3322
反应条件
1: toluene / 1 h / 100 °C
2: cyclohexane / 1 h / 250 °C
View Scheme
参考文献
Thomas, Alan F.; Perret, Celia
Tetrahedron, 1986 , vol. 42, # 12 p. 3311 - 3322
反应条件
sulfuric acid in methanol
T=25°C; Kinetics; Further Variations:reagent concentrations;
参考文献
Pytela, Oldrich; Trlida, Bronislav
Collection of Czechoslovak Chemical Communications, 2007 , vol. 72, # 8 p. 1025 - 1036
反应条件
sodium hydrogencarbonate
参考文献
Monsanto Chem.Co.
Patent: US2634294 , 1950 ;
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran
Decomposition; rearrangement; Product distribution; Further Variations:TemperaturesReagents;
参考文献
Bradley; Williams; Blann, Kevin; Holzapfel, Cedric W.
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2834 - 2836
反应条件
potassium hydrogensulfate
unter vermindertem Druck;
参考文献
Jiang, Xi-Kui; Liu, Wayne Wei-Zhong; Wu, Shi-Hui
Journal of Physical Organic Chemistry, 1994 , vol. 7, p. 96 - 104