1,2-二溴-4,5-二硝基苯合成路线 （共 6 条）
反应条件
hydrogenchloride; tin in ethanol
参考文献
Moerkved, Eva H.; Neset, Siren M.; Bjoerlo, Olav; Kjoesen, Helge; Hvistendahl, Georg; Mo, Frode
Acta Chemica Scandinavica, 1995 , vol. 49, # 9 p. 658 - 662
反应条件
hydrogenchloride; tin
参考文献
Woolley; Pringle
Journal of Biological Chemistry, 1952 , vol. 194, p. 729,734
反应条件
(i) H2, Raney-Ni, THF, (ii) PhNSO, toluene; Multistep reaction;
参考文献
Moerkved, Eva H.; Neset, Siren M.; Bjoerlo, Olav; Kjoesen, Helge; Hvistendahl, Georg; Mo, Frode
Acta Chemica Scandinavica, 1995 , vol. 49, # 9 p. 658 - 662
反应条件
hydrogenchloride; tin
参考文献
Woolley; Pringle
Journal of Biological Chemistry, 1952 , vol. 194, p. 729,734
反应条件
1: 42 percent / NH3 / ethanol 2: 54 percent / dimethylformamide; nitrobenzene / 4.5 h / 180 °C 3: 70 percent / SnCl2 / 0.33 h / 70 °C View Scheme
参考文献
Rusanova, Julia; Pilkington, Melanie; Decurtins, Silvio
Chemical Communications, 2002 , # 19 p. 2236 - 2237
反应条件
1: 72 percent / CuI; Pd(PPh3)4; Et3N / tetrahydrofuran / 90 h / 20 °C
2: 90 percent / hydrazine hydrate; Pd/C / ethanol / 4 h / Heating
View Scheme
参考文献
Zhang, Fan; Bai, Shi; Yap, Glenn P. A.; Tarwade, Vinod; Fox, Joseph M.
Journal of the American Chemical Society, 2005 , vol. 127, # 30 p. 10590 - 10599
