5-甲基四氢呋喃-2,4-二酮合成路线 （共 1 条）
反应条件
1.1: 85 percent / Et3N; 4-dimethylaminopyridine; dicyclohexylcarbodiimide / CH2Cl2 / 15 h / 0 - 20 °C 2.1: 80 percent / NaBH3CN / acetic acid / 5 h / 20 °C 3.1: 89 percent / toluene / Heating 4.1: aq. HCl; NaBH3CN / methanol 4.2: NaOH / H2O; diethyl ether 5.1: SiO2 / toluene / Heating View Scheme
参考文献
Pashkovskii; Katok; Khlebnikova; Koroleva; Lakhvich
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 7 p. 998 - 1009
