T=750°C; P=0.003 Torr; 2.77778E-07 h; Further byproducts given;
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
T=750°C; P=0.003 Torr; 2.77778E-07 h; Further byproducts given;
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: 62 percent / anhydrous hydrazine / dioxane / 40 h / Heating
2: nickel peroxide
3: 21 percent / tetrahydrofuran / 0 °C
4: 0.67 h / 160 °C
5: trimethyl phosphite / 1 h / 60 °C
6: 0 h / 650 °C / 0 - 0 Torr
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: nickel peroxide
2: 21 percent / tetrahydrofuran / 0 °C
3: 0.67 h / 160 °C
4: trimethyl phosphite / 1 h / 60 °C
5: 0 h / 650 °C / 0 - 0 Torr
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: 21 percent / tetrahydrofuran / 0 °C
2: 0.67 h / 160 °C
3: trimethyl phosphite / 1 h / 60 °C
4: 0 h / 650 °C / 0 - 0 Torr
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: 79 percent / diethyl ether / 48 h / Ambient temperature
2: 88 percent / trimethyl phosphite / CHCl3 / 48 h / Heating
3: 75 percent / benzene / 18 h / Irradiation
4: 78 percent / diethyl ether / 1.5 h
5: potassium hydrogen sulphate / 0.5 h / 80 °C / 10 Torr
View Scheme
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
1: 78 percent / diethyl ether / 1.5 h
2: potassium hydrogen sulphate / 0.5 h / 80 °C / 10 Torr
View Scheme
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
1: 75 percent / benzene / 18 h / Irradiation
2: 78 percent / diethyl ether / 1.5 h
3: potassium hydrogen sulphate / 0.5 h / 80 °C / 10 Torr
View Scheme
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
