1: 88 percent / trimethyl phosphite / CHCl3 / 48 h / Heating
2: 75 percent / benzene / 18 h / Irradiation
3: 78 percent / diethyl ether / 1.5 h
4: potassium hydrogen sulphate / 0.5 h / 80 °C / 10 Torr
View Scheme
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: trimethyl phosphite / 1 h / 60 °C
2: 0 h / 650 °C / 0 - 0 Torr
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
1: 0.67 h / 160 °C
2: trimethyl phosphite / 1 h / 60 °C
3: 0 h / 650 °C / 0 - 0 Torr
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
sodium hydroxide in 1,2-dichloro-benzene
heating in vac.; Mechanism;
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
hydrogen; palladium on activated charcoal in methanol
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
