2,5-二甲基-3,4-二(1-甲基乙基)-2,4-己二烯合成路线 （共 11 条）
反应条件
1: 80 h / 225 °C
2: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 64 percent Chromat. / 0 h / 570 °C / 0 - 0.01 Torr
2: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 62 percent / anhydrous hydrazine / dioxane / 40 h / Heating
2: nickel peroxide
3: 21 percent / tetrahydrofuran / 0 °C
4: 0.67 h / 160 °C
5: trimethyl phosphite / 1 h / 60 °C
6: 0 h / 650 °C / 0 - 0 Torr
7: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 0 h / 600 °C / 0 - 0 Torr
2: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: nickel peroxide
2: 21 percent / tetrahydrofuran / 0 °C
3: 0.67 h / 160 °C
4: trimethyl phosphite / 1 h / 60 °C
5: 0 h / 650 °C / 0 - 0 Torr
6: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 21 percent / tetrahydrofuran / 0 °C
2: 0.67 h / 160 °C
3: trimethyl phosphite / 1 h / 60 °C
4: 0 h / 650 °C / 0 - 0 Torr
5: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 0 h / 650 °C / 0 - 0 Torr
2: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: trimethyl phosphite / 1 h / 60 °C
2: 0 h / 650 °C / 0 - 0 Torr
3: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
反应条件
1: 0.67 h / 160 °C
2: trimethyl phosphite / 1 h / 60 °C
3: 0 h / 650 °C / 0 - 0 Torr
4: hydrogen / 10percent palladium on charcoal / methanol
View Scheme
参考文献
Bushby, Richard J.; Mann, Stephen; Jesudason, Malini, V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2457 - 2464
