甲基丙烯酰氧甲基三甲氧基硅烷合成路线 (共 3 条)
反应条件
1: 2-methyl-2-propenoic acid With potassium hydroxide in toluene 2: (chloromethyl)trimethoxysilane With 4,4'-bismethylene(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in toluene; butanone T=110°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1081 - 1092
反应条件
1,1-bis (3,5-di-t-butyl-4-hydroxyphenyl)-methane
参考文献
US2004/171859 A1, ;
Page 4-5 ;
反应条件
1: With acetic acid; trifluorormethanesulfonic acid T=45°C; 2 h; 2: With acetyl chloride T=40°C; 0.333333 h; 3: With 1,1,1,3,3,3-hexamethyl-disilazane
参考文献
WACKER CHEMIE AG
Patent: US2010/41909 A1, 2010 ;
Location in patent: Page/Page column 6 ;