2,2’-二硫二苯甲酸二甲酯合成路线 （共 34 条）
反应条件
in dichloromethane
T=0°C; 0.5 h;
参考文献
Hunter, Roger; Caira, Mino; Stellenboom, Nashia
Journal of Organic Chemistry, 2006 , vol. 71, # 21 p. 8268 - 8271
反应条件
triethylamine in tetrahydrofuran
10 h; Heating;
参考文献
Shimizu, Masao; Fukazawa, Hidenori; Inoue, Jun'ichi; Abe, Yoshimoto; Konakahara, Takeo
Heterocycles, 2007 , vol. 71, # 1 p. 61 - 73
反应条件
in dichloromethane
T=-196 - 20°C; 0.166667 h;
参考文献
Wentrup, Curt; Bender, Harald; Gross, Gerhard
Journal of Organic Chemistry, 1987 , vol. 52, # 17 p. 3838 - 3847
反应条件
sodium hydroxide
T=25°C; 3 h;
参考文献
Jin, Chun Keun; Moon, Jung-Kyen; Lee, Woo Song; Nam, Keun Soo
Synlett, 2003 , # 13 p. 1967 - 1968
参考文献
Gilman; Arntzen; Webb
Journal of Organic Chemistry, 1945 , vol. 10, p. 374,378
Full Text Show Details
Gilman; Webb
Journal of the American Chemical Society, 1949 , vol. 71, p. 4062,4063
反应条件
1: 620 °C / 0 Torr
2: 2.) O2 / 1.) CH2Cl2, from -196 deg C to 20 deg C, 10 min, 2.) CH2Cl2, RT, 12 h
View Scheme
参考文献
Wentrup, Curt; Bender, Harald; Gross, Gerhard
Journal of Organic Chemistry, 1987 , vol. 52, # 17 p. 3838 - 3847
反应条件
in toluene
72 h; Heating;
参考文献
Davis, Franklin A.; Jenkins, Linda A.; Billmers, Robert L.
Journal of Organic Chemistry, 1986 , vol. 51, # 7 p. 1033 - 1040
反应条件
1: tin dichloride; concentrated hydrochloric acid; water
2: hydrogen chloride
View Scheme
参考文献
Gattermann
Chemische Berichte, 1899 , vol. 32, p. 1156
参考文献
List; Stein
Chemische Berichte, 1898 , vol. 31, p. 1668
反应条件
1: hydrogen chloride
2: FeCl3; alcohol
View Scheme
参考文献
Gattermann
Chemische Berichte, 1899 , vol. 32, p. 1156
