反应条件
1: (1S,2R,8R)-8,11,11-trimethyl-3-oxa-6-azatricyclo[6.2.1.02,7]-undec-6-en-4-one With lithium diisopropyl amide in tetrahydrofuran T=-30°C; 1.5 h; 2: allyl bromide With N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran T=-78°C; 14 h; 3: With hydrogenchloride T=87°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 2 p. 658 - 661
