N-(3-溴丙基)苯二胺合成路线 （共 93 条）
反应条件
tetrabutylammomium bromide; potassium carbonate T=20°C; 1 h; Neat (no solvent);
参考文献
Jaskowska, Jolanta; Kowalski, Piotr
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 5 p. 1371 - 1375
反应条件
1: With diisopropyl-carbodiimide; copper(II) bis(trifluoromethanesulfonate) in tetrahydrofuran T=100°C; 0.0833333 h; microwave irradiation; 2: With acetyl-bromide in tetrahydrofuran T=150°C; 0.0833333 h; microwave irradiation; Further stages.;
参考文献
Crosignani, Stefano; Nadal, Brice; Li, Zhengning; Linclau, Bruno
Chemical Communications, 2003 , # 2 p. 260 - 261
反应条件
in N,N-dimethyl-formamide T=20°C; Gabriel Amine Synthesis; 24 h; Inert atmosphere;
参考文献
Gauchot, Vincent; Branca, Mathieu; Schmitzer, Andreea
Chemistry - A European Journal, 2014 , vol. 20, # 6 p. 1530 - 1538
反应条件
sodium hydroxide in N,N-dimethyl-formamide
参考文献
Chen, Gang; Crawford, Jason; Skerlj, Renato
Patent: US2005/154201 A1, 2005 ;
参考文献
Chemische Berichte, , vol. 38, p. 2394
反应条件
anschliessenden Erwaermen mit Phosphor(III)-bromid;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 78, p. 289,309
Canadian Journal of Chemistry, , vol. 31, p. 1060,1061
参考文献
Chemische Berichte, , vol. 42, p. 2052
参考文献
Chemische Berichte, , vol. 38, p. 2394
反应条件
Ni(0)*2EC*Py complex in acetonitrile T=20°C; 4 h; Inert atmosphere;
参考文献
Peng, Yu; Luo, Long; Yan, Chang-Song; Zhang, Jian-Jian; Wang, Ya-Wen
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10960 - 10967
反应条件
[Ni0(1,5-cyclooctadiene)2]; zinc; (4-Cl)-H-PyBox in N,N-dimethyl acetamide T=25°C; 16 h; Inert atmosphere;
参考文献
Yu, Xiaolong; Yang, Tao; Wang, Shulin; Xu, Hailiang; Gong, Hegui
Organic Letters, 2011 , vol. 13, # 8 p. 2138 - 2141
